About: Chloride present in biological samples as a tool for enhancement of sensitivity in CZE analysis of trace analytes.

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About: Chloride present in biological samples as a tool for enhancement of sensitivity in CZE analysis of trace analytes. Goto Sponge NotDistinct Permalink

An Entity of Type : http://linked.opendata.cz/ontology/domain/vavai/Vysledek, within Data Space : linked.opendata.cz associated with source document(s)

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Having acetoacetate, malate, citrate and some drug metabolites in untreated serum samples, the stacking mechanism of these compounds in an electrolyte system comprising 5 mM mandelic acid and e-aminocaproic acid (pH 3.8) is explained. Analytes are monitored by indirect UV absorption detection. Attention is paid to the minimum chloride concentration required with respect to the concentration ratio of phosphate (stacker) and lactate (destacker) present in the sample so as to ensure both stacking and separation of trace analytes. Insight into the separation process is given both with computer simulations and experiments. For selected analytes, the effect of the chloride concentration on quantitative evaluation, sensitivity and limit of detection is demonstrated as well. Having acetoacetate, malate, citrate and some drug metabolites in untreated serum samples, the stacking mechanism of these compounds in an electrolyte system comprising 5 mM mandelic acid and e-aminocaproic acid (pH 3.8) is explained. Analytes are monitored by indirect UV absorption detection. Attention is paid to the minimum chloride concentration required with respect to the concentration ratio of phosphate (stacker) and lactate (destacker) present in the sample so as to ensure both stacking and separation of trace analytes. Insight into the separation process is given both with computer simulations and experiments. For selected analytes, the effect of the chloride concentration on quantitative evaluation, sensitivity and limit of detection is demonstrated as well. (en)
Title	Chloride present in biological samples as a tool for enhancement of sensitivity in CZE analysis of trace analytes. Chloride present in biological samples as a tool for enhancement of sensitivity in CZE analysis of trace analytes. (en)
skos:prefLabel	Chloride present in biological samples as a tool for enhancement of sensitivity in CZE analysis of trace analytes. Chloride present in biological samples as a tool for enhancement of sensitivity in CZE analysis of trace analytes. (en)
skos:notation	RIV/68081715:_____/01:25010054!RIV/2003/AV0/A25003/N
http://linked.open.../vavai/riv/strany	97
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(GA203/99/0044), P(IAA4031703), Z(AV0Z4031919)
http://linked.open...vai/riv/dodaniDat	2003
http://linked.open...aciTvurceVysledku	Boček, Petr Křivánková, Ludmila Gebauer, Petr Pantůčková, Pavla
http://linked.open.../riv/druhVysledku	D - Článek ve sborníku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Ústav analytické chemie AV ČR, v. v. i.
http://linked.open...dnocenehoVysledku	675555
http://linked.open...ai/riv/idVysledku	RIV/68081715:_____/01:25010054
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	capillary zone electrophoresis; transient isotachophoresis; stacking effect (en)
http://linked.open.../riv/klicoveSlovo	transient isotachophoresis capillary zone electrophoresis stacking effect
http://linked.open...ontrolniKodProRIV	[88B62B765B31]
http://linked.open...v/mistoKonaniAkce	Verona [IT]
http://linked.open...i/riv/mistoVydani	Verona
http://linked.open...i/riv/nazevZdroje	ICES 2001: An Electrophoretic Odyssey.
http://linked.open...in/vavai/riv/obor	CB
http://linked.open...ichTvurcuVysledku	4 (xsd:int)
http://linked.open...cetTvurcuVysledku	5 (xsd:int)
http://linked.open...ocetUcastnikuAkce	0 (xsd:int)
http://linked.open...nichUcastnikuAkce	0 (xsd:int)
http://linked.open...vavai/riv/projekt	The use of new analytical instrumentation in research of analytical and diagnostic methods Methodology of analytical electrophoresis of samples with complex matrices
http://linked.open...UplatneniVysledku	2001
http://linked.open...iv/tvurceVysledku	Boček, Petr Křivánková, Ludmila Gebauer, Petr Pantůčková, Pavla Thormann, W.
http://linked.open...vavai/riv/typAkce	EUR - Evropská
http://linked.open.../riv/zahajeniAkce	2001-06-10 (xsd:date)
http://linked.open...n/vavai/riv/zamer	Vyvinutí nových metod analytické chemie pro potřeby společenské praxe
number of pages	1 (xsd:int)
http://purl.org/ne...btex#hasPublisher	Neuveden

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