About: Determination of Total Sulfur in Fifteen Geological Materials Using Inductively Coupled Plasma-Optical Emission Spectrometry (ICP-OES) and Combustion/Infrared Spectrometry     Goto   Sponge   NotDistinct   Permalink

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  • A method for the determination of total sulfur in geological materials by inductively coupled plasma-optical emission spectrometry (ICP-OES) is described. We show that good results were obtained using this method even for sample types with very low (< 20 μg g1) sulfur concentration (e.g., peridotite). Sulfur was determined in fifteen geological reference materials with different sulfur contents. For reference materials with certified sulfur contents, the ICP-OES method gave results in excellent agreement with certified values, and uncertainties better than 4% RSD. ICP-OES results for sulfur in other reference materials yielded RSDs better than 10%, where S concentrations were > 100 μg g1 (except for diabase W-2a, 16% RSD). Reference materials with lower sulfur contents (< 40 μg g1) showed much higher RSDs (17–18%). Except for RMs with certified values for sulfur, most data obtained by the combustion infrared detection method generally showed higher concentrations than those measured by ICP-OES and a better RSD ( 8% for all materials except DTS-2b).
  • A method for the determination of total sulfur in geological materials by inductively coupled plasma-optical emission spectrometry (ICP-OES) is described. We show that good results were obtained using this method even for sample types with very low (< 20 μg g1) sulfur concentration (e.g., peridotite). Sulfur was determined in fifteen geological reference materials with different sulfur contents. For reference materials with certified sulfur contents, the ICP-OES method gave results in excellent agreement with certified values, and uncertainties better than 4% RSD. ICP-OES results for sulfur in other reference materials yielded RSDs better than 10%, where S concentrations were > 100 μg g1 (except for diabase W-2a, 16% RSD). Reference materials with lower sulfur contents (< 40 μg g1) showed much higher RSDs (17–18%). Except for RMs with certified values for sulfur, most data obtained by the combustion infrared detection method generally showed higher concentrations than those measured by ICP-OES and a better RSD ( 8% for all materials except DTS-2b). (en)
Title
  • Determination of Total Sulfur in Fifteen Geological Materials Using Inductively Coupled Plasma-Optical Emission Spectrometry (ICP-OES) and Combustion/Infrared Spectrometry
  • Determination of Total Sulfur in Fifteen Geological Materials Using Inductively Coupled Plasma-Optical Emission Spectrometry (ICP-OES) and Combustion/Infrared Spectrometry (en)
skos:prefLabel
  • Determination of Total Sulfur in Fifteen Geological Materials Using Inductively Coupled Plasma-Optical Emission Spectrometry (ICP-OES) and Combustion/Infrared Spectrometry
  • Determination of Total Sulfur in Fifteen Geological Materials Using Inductively Coupled Plasma-Optical Emission Spectrometry (ICP-OES) and Combustion/Infrared Spectrometry (en)
skos:notation
  • RIV/67985831:_____/12:00388152!RIV13-AV0-67985831
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  • I, P(KJB300130612), Z(AV0Z30130516), Z(MSM0021620855)
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  • 4
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  • 130661
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  • RIV/67985831:_____/12:00388152
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  • sulfur; ICP-OES; combustion; infrared detection; reference materials (en)
http://linked.open.../riv/klicoveSlovo
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  • FR - Francouzská republika
http://linked.open...ontrolniKodProRIV
  • [B35129636F3D]
http://linked.open...i/riv/nazevZdroje
  • Geostandards and Geoanalytical Research
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  • 36
http://linked.open...iv/tvurceVysledku
  • Rohovec, Jan
  • Ackerman, Lukáš
  • Šebek, O.
http://linked.open...ain/vavai/riv/wos
  • 000314395900004
http://linked.open...n/vavai/riv/zamer
issn
  • 1639-4488
number of pages
http://bibframe.org/vocab/doi
  • 10.1111/j.1751-908X.2012.00144.x
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