About: In position 7 l- and d-Tic-substituted oxytocin and deamino oxytocin: NMR study and conformational insights     Goto   Sponge   NotDistinct   Permalink

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  • NMR study (NOESY, TOCSY, H-1-C-13 HSQC spectra) of analogues of oxytocin and deaminoocytocin having in position 7 L- or D-Tic is presented. The existence of both cis and trans configurations of the Cys(6)-D-Tic(7) bond is supported by observation of two sets of cross-peaks for H-1 and C-13 nuclei for most of the residues of the peptide not only in NOESY and TOCSY but also in H-1-C-13 HSQC spectra. The MS and HPLC indicate the presence of a single molecule/peptide, and NMR data thus suggest that this second set of peaks is due to the cis conformation.
  • NMR study (NOESY, TOCSY, H-1-C-13 HSQC spectra) of analogues of oxytocin and deaminoocytocin having in position 7 L- or D-Tic is presented. The existence of both cis and trans configurations of the Cys(6)-D-Tic(7) bond is supported by observation of two sets of cross-peaks for H-1 and C-13 nuclei for most of the residues of the peptide not only in NOESY and TOCSY but also in H-1-C-13 HSQC spectra. The MS and HPLC indicate the presence of a single molecule/peptide, and NMR data thus suggest that this second set of peaks is due to the cis conformation. (en)
Title
  • In position 7 l- and d-Tic-substituted oxytocin and deamino oxytocin: NMR study and conformational insights
  • In position 7 l- and d-Tic-substituted oxytocin and deamino oxytocin: NMR study and conformational insights (en)
skos:prefLabel
  • In position 7 l- and d-Tic-substituted oxytocin and deamino oxytocin: NMR study and conformational insights
  • In position 7 l- and d-Tic-substituted oxytocin and deamino oxytocin: NMR study and conformational insights (en)
skos:notation
  • RIV/61388963:_____/10:00347360!RIV11-AV0-61388963
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(AV0Z40550506)
http://linked.open...iv/cisloPeriodika
  • 2
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 263273
http://linked.open...ai/riv/idVysledku
  • RIV/61388963:_____/10:00347360
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • oxytocin analogues; deaminooxytocin; NMR (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • AT - Rakouská republika
http://linked.open...ontrolniKodProRIV
  • [786FA1DC24B2]
http://linked.open...i/riv/nazevZdroje
  • Amino Acids
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 39
http://linked.open...iv/tvurceVysledku
  • Borovičková, Lenka
  • Slaninová, Jiřina
  • Cordopatis, P.
  • Fragiadaki, M.
  • Magafa, V.
  • Spyranti, Z.
  • Spyroulias, G. A.
http://linked.open...ain/vavai/riv/wos
  • 000279190400024
http://linked.open...n/vavai/riv/zamer
issn
  • 0939-4451
number of pages
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