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Description
  • o-Phthaldialdehyde in combination with the series of 6 thiosugars were used for the pre-column chiral derivatization of selected primary amino acids. The diastereomers were resolved on conventional reversed-phase column and with fluorescence detection. A surprisingly effective resolution of 1-isoindolyl(1-thioglycosides) derived from 1-thio-β-L-fucose was observed.
  • o-Phthaldialdehyde in combination with the series of 6 thiosugars were used for the pre-column chiral derivatization of selected primary amino acids. The diastereomers were resolved on conventional reversed-phase column and with fluorescence detection. A surprisingly effective resolution of 1-isoindolyl(1-thioglycosides) derived from 1-thio-β-L-fucose was observed. (en)
  • Pro předkolonovou chirální derivatizaci vybraných primárních aminokyselin byl použit o-ftaldialdehyd v kombinaci se sérií šesti thiocukrů. Vzniklé diastereoisomery byly separovány na konvenční koloně s reverzní fází s využitím fluorescenčního detektoru. Bylo pozorováno překvapivě účinné rozlišení 1-isoindolyl(1-thioglycosidů) odvozených od 1-thio-β-L-fucosy. (cs)
Title
  • Thiosugars – Derivatization agents for the chiral resolution of homoleucines
  • Thiosugars – Derivatization agents for the chiral resolution of homoleucines (en)
  • Thiocukry – Derivatizační činidla pro chirální separaci homoleucinů (cs)
skos:prefLabel
  • Thiosugars – Derivatization agents for the chiral resolution of homoleucines
  • Thiosugars – Derivatization agents for the chiral resolution of homoleucines (en)
  • Thiocukry – Derivatizační činidla pro chirální separaci homoleucinů (cs)
skos:notation
  • RIV/60077344:_____/08:00098885!RIV08-AV0-60077344
http://linked.open.../vavai/riv/strany
  • 133;136
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GA303/06/1674), Z(AV0Z50070508)
http://linked.open...iv/cisloPeriodika
  • 1
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 399978
http://linked.open...ai/riv/idVysledku
  • RIV/60077344:_____/08:00098885
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • amino acids; chiral separation; thiosugars-OPA derivatization (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV
  • [3D8304082BAE]
http://linked.open...i/riv/nazevZdroje
  • Journal of Separation Science
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 31
http://linked.open...iv/tvurceVysledku
  • Zahradníčková, Helena
  • Jegorov, A.
  • Zelenka, K.
  • Trnka, T.
http://linked.open...n/vavai/riv/zamer
issn
  • 1615-9306
number of pages
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