About: <sup>15</sup>N NMR Spectroscopy in Structural Analysis: An Update (2001-2005)

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Since our previous review article (Curr. Org. Chem. 2002, 6, 35), significant improvements and an array of 15N NMR applications in structural analysis have been published. This report aims to update coverage of improvements in methodology and various types of applications published over the period 2001 - 2005. Substantial progress in cryogenic probe technology and the commercial availability of cryoprobes have facilitated the measurement of 15N NMR parameters. The number of solid-state applications has increased significantly during the past few years. In contrast to our previous review, this article covers 15N solid-state studies. The 15N NMR chemical shifts of organic molecules are routinely measured by using cross-polarization magic-angle spinning (CP/MAS) techniques. The principal values of the chemical shift tensors can also be determined. 1H-15N and 2H-15N distance measurements made by means of 1H detection are currently used in NMR crystallography. Since our previous review article (Curr. Org. Chem. 2002, 6, 35), significant improvements and an array of 15N NMR applications in structural analysis have been published. This report aims to update coverage of improvements in methodology and various types of applications published over the period 2001 - 2005. Substantial progress in cryogenic probe technology and the commercial availability of cryoprobes have facilitated the measurement of 15N NMR parameters. The number of solid-state applications has increased significantly during the past few years. In contrast to our previous review, this article covers 15N solid-state studies. The 15N NMR chemical shifts of organic molecules are routinely measured by using cross-polarization magic-angle spinning (CP/MAS) techniques. The principal values of the chemical shift tensors can also be determined. 1H-15N and 2H-15N distance measurements made by means of 1H detection are currently used in NMR crystallography. (en)
Title	¹⁵N NMR Spectroscopy in Structural Analysis: An Update (2001-2005) ¹⁵N NMR Spectroscopy in Structural Analysis: An Update (2001-2005) (en)
skos:prefLabel	¹⁵N NMR Spectroscopy in Structural Analysis: An Update (2001-2005) ¹⁵N NMR Spectroscopy in Structural Analysis: An Update (2001-2005) (en)
skos:notation	RIV/00216224:14310/07:00022182!RIV10-MSM-14310___
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(LC06030), Z(MSM0021622410), Z(MSM0021622413)
http://linked.open...iv/cisloPeriodika	13
http://linked.open...vai/riv/dodaniDat	2010
http://linked.open...aciTvurceVysledku	Toušek, Jaromír Marek, Radek
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Masarykova univerzita / Přírodovědecká fakulta
http://linked.open...dnocenehoVysledku	453565
http://linked.open...ai/riv/idVysledku	RIV/00216224:14310/07:00022182
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	15N NMR spectroscopy; inverse detection; CP/MAS; quantum chemical calculations; 15N chemical shift tensor; hydrogen bonding; tautomerism; complexation (en)
http://linked.open.../riv/klicoveSlovo	CP/MAS inverse detection hydrogen bonding 15N NMR spectroscopy quantum chemical calculations complexation tautomerism 15N chemical shift tensor
http://linked.open...odStatuVydavatele	NL - Nizozemsko
http://linked.open...ontrolniKodProRIV	[2A96B3BA1ACD]
http://linked.open...i/riv/nazevZdroje	Current Organic Chemistry
http://linked.open...in/vavai/riv/obor	CC
http://linked.open...ichTvurcuVysledku	2 (xsd:int)
http://linked.open...cetTvurcuVysledku	5 (xsd:int)
http://linked.open...vavai/riv/projekt	Biomolecular centre
http://linked.open...UplatneniVysledku	2007
http://linked.open...v/svazekPeriodika	11
http://linked.open...iv/tvurceVysledku	Marek, Radek Lyčka, Antonín Sievänen, Elina Toušek, Jaromír Kolehmainen, Erkki
http://linked.open...n/vavai/riv/zamer	Proteiny v metabolismu a při interakci organismů s prostředím Physical and chemical properties of advanced materials and structures
issn	1385-2728
number of pages	52 (xsd:int)
http://localhost/t...ganizacniJednotka	14310
is http://linked.open...avai/riv/vysledek of	<sup>15</sup>N NMR Spectroscopy in Structural Analysis: An Update (2001-2005) <sup>15</sup>N NMR Spectroscopy in Structural Analysis: An Update (2001-2005) <sup>15</sup>N NMR Spectroscopy in Structural Analysis: An Update (2001-2005)

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