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  • The structure of the quaternary tetrahydroprotoberberine alkaloid escholidine is revised on the basis of 2D NMR spectroscopy and X-ray diffraction. In contrast to the originally reported constitution, escholidine bears an -OH group at C-9 and an -OCH3 group at C-10. The 1H and 13C NMR data and long-range 1H-13C and NOE interactions of escholidine are compared with those of thalifendine and tetrahydroberberrubine. The 15N NMR data of escholidine obtained by using long-range 1H-15N correlation experiments at natural abundance are also reported.
  • The structure of the quaternary tetrahydroprotoberberine alkaloid escholidine is revised on the basis of 2D NMR spectroscopy and X-ray diffraction. In contrast to the originally reported constitution, escholidine bears an -OH group at C-9 and an -OCH3 group at C-10. The 1H and 13C NMR data and long-range 1H-13C and NOE interactions of escholidine are compared with those of thalifendine and tetrahydroberberrubine. The 15N NMR data of escholidine obtained by using long-range 1H-15N correlation experiments at natural abundance are also reported. (en)
Title
  • Revision of the Structure of Escholidine
  • Revision of the Structure of Escholidine (en)
skos:prefLabel
  • Revision of the Structure of Escholidine
  • Revision of the Structure of Escholidine (en)
skos:notation
  • RIV/00216224:14310/06:00016909!RIV10-MSM-14310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(LC06030), Z(MSM0021622413)
http://linked.open...iv/cisloPeriodika
  • 6
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 497504
http://linked.open...ai/riv/idVysledku
  • RIV/00216224:14310/06:00016909
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • alkaloid; escholidine; NMR; X-ray (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • US - Spojené státy americké
http://linked.open...ontrolniKodProRIV
  • [8D46E878DE49]
http://linked.open...i/riv/nazevZdroje
  • Journal of Natural Products
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 69
http://linked.open...iv/tvurceVysledku
  • Dostál, Jiří
  • Marek, Radek
  • Nečas, Marek
  • Slavík, Jiří
  • Chudík, Stanislav
  • Sečkářová, Pavlína
http://linked.open...ain/vavai/riv/wos
  • 000238478800017
http://linked.open...n/vavai/riv/zamer
issn
  • 0163-3864
number of pages
http://localhost/t...ganizacniJednotka
  • 14310
is http://linked.open...avai/riv/vysledek of
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