About: Synthesis of galactosyl phosphonate and methylphosphonate     Goto   Sponge   NotDistinct   Permalink

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  • Methyl galactopyranoside was converted to the 1-phosphonate by a reaction pathway consisted of protection of all hydroxyl groups, the transformation of 1-methoxyl group into acetate and final nucleophilic substitution with triethylphosphite. The reactionsequence was closed by the deprotection step. Both anomeric phosphonate were obtained, separated and identified by NMR, optical rotation and MS data.
  • Methyl galactopyranoside was converted to the 1-phosphonate by a reaction pathway consisted of protection of all hydroxyl groups, the transformation of 1-methoxyl group into acetate and final nucleophilic substitution with triethylphosphite. The reactionsequence was closed by the deprotection step. Both anomeric phosphonate were obtained, separated and identified by NMR, optical rotation and MS data. (en)
Title
  • Synthesis of galactosyl phosphonate and methylphosphonate
  • Synthesis of galactosyl phosphonate and methylphosphonate (en)
skos:prefLabel
  • Synthesis of galactosyl phosphonate and methylphosphonate
  • Synthesis of galactosyl phosphonate and methylphosphonate (en)
skos:notation
  • RIV/60461373:22330/02:00006855!RIV/2004/MSM/223304/N
http://linked.open.../vavai/riv/strany
  • 12
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  • Z(MSM 223300006)
http://linked.open...vai/riv/dodaniDat
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  • 666168
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  • RIV/60461373:22330/02:00006855
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  • galaktosyltransferases, phosphonate, galactoside, inhibitor (en)
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  • [824721C5DA4C]
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  • Praha
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  • Praha
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  • Imberty, Anne
  • Moravcová, Jitka
  • Kočalka, Petr
  • Heissigerová, Helena
http://linked.open...vavai/riv/typAkce
http://linked.open.../riv/zahajeniAkce
http://linked.open...n/vavai/riv/zamer
number of pages
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  • Česká chemická společnost
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  • 80-86238-20-2
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  • 22330
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