About: Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry.

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	The objective of the presented study was to develop and optimize a simple, high-throughput method for the control of 32 mycotoxins (Fusarium and Alternaria toxins, aflatoxins, ergot alkaloids, ochratoxins, and sterigmatocystin) in beer. Due to the broad range of their physicochemical properties, the sample preparation step was simplified as much as possible to avoid analyte losses. The addition of acetonitrile to beer samples enabled precipitation of abundant matrix components. The clean-up efficiency was controlled by ambientmass spectrometry employing a direct analysis in real time (DART) ion source. For determination of analytes, ultra-high-performance liquid chromatogramy hyphenated with high-resolution mass spectrometry utilizing an orbitrap (U-HPLC?orbitrapMS) or time-of-flight (TOFMS) technology was used. Because of significantly better detection capabilities of the orbitrap technology, the U-HPLC?orbitrapMSmethod was chosen as a determinative step and fully validated. To compensate matrix The objective of the presented study was to develop and optimize a simple, high-throughput method for the control of 32 mycotoxins (Fusarium and Alternaria toxins, aflatoxins, ergot alkaloids, ochratoxins, and sterigmatocystin) in beer. Due to the broad range of their physicochemical properties, the sample preparation step was simplified as much as possible to avoid analyte losses. The addition of acetonitrile to beer samples enabled precipitation of abundant matrix components. The clean-up efficiency was controlled by ambientmass spectrometry employing a direct analysis in real time (DART) ion source. For determination of analytes, ultra-high-performance liquid chromatogramy hyphenated with high-resolution mass spectrometry utilizing an orbitrap (U-HPLC?orbitrapMS) or time-of-flight (TOFMS) technology was used. Because of significantly better detection capabilities of the orbitrap technology, the U-HPLC?orbitrapMSmethod was chosen as a determinative step and fully validated. To compensate matrix (en)
Title	Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry. Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry. (en)
skos:prefLabel	Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry. Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry. (en)
skos:notation	RIV/60461373:22330/10:00024320!RIV11-MSM-22330___
http://linked.open...avai/riv/aktivita	P R Z
http://linked.open...avai/riv/aktivity	P(1M0570), P(2B08049), R, Z(MSM6046137305)
http://linked.open...iv/cisloPeriodika	22
http://linked.open...vai/riv/dodaniDat	2011
http://linked.open...aciTvurceVysledku	Zachariášová, Milena Vepříková, Zdenka Malachová, Alexandra Čajka, Tomáš Hajšlová, Jana
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Vysoká škola chemicko-technologická v Praze / Fakulta potravinářské a biochemické technologie
http://linked.open...dnocenehoVysledku	246427
http://linked.open...ai/riv/idVysledku	RIV/60461373:22330/10:00024320
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	mycotoxins; beer; high resolution mass spectrometry (en)
http://linked.open.../riv/klicoveSlovo	beer high resolution mass spectrometry mycotoxins
http://linked.open...odStatuVydavatele	GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV	[2D4AE3DDBBBD]
http://linked.open...i/riv/nazevZdroje	Rapid Communications in Mass Spectrometry
http://linked.open...in/vavai/riv/obor	GM
http://linked.open...ichTvurcuVysledku	5 (xsd:int)
http://linked.open...cetTvurcuVysledku	6 (xsd:int)
http://linked.open...vavai/riv/projekt	Research Centre for Study of Extract Compounds of Barley and Hop Free and bound forms of fusarium mycotoxins in cereals and processed products; strategy of control and minimisation.
http://linked.open...UplatneniVysledku	2010
http://linked.open...v/svazekPeriodika	24
http://linked.open...iv/tvurceVysledku	Hajšlová, Jana Zachariášová, Milena Čajka, Tomáš Godula, Michal Vepříková, Zdenka Krplová, Alexandra
http://linked.open...ain/vavai/riv/wos	000284023400018
http://linked.open...n/vavai/riv/zamer	Teoretické základy potravinářských a biochemických technologií
issn	0951-4198
number of pages	11 (xsd:int)
http://localhost/t...ganizacniJednotka	22330
is http://linked.open...avai/riv/vysledek of	Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry. Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry. Analysis of multiple mycotoxins in beer employing (ultra)-high resolution mass spectrometry.

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