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  • This paper deals with the preparation of a variously substituted non-symmetrical azine set. The starting molecule for their preparation was a protected hydrazone. The protection was performed applying Zwierzak’s method. This procedure is based on the transfer of hydrazine to diethyl-hydrazidophosphate, which reacts with aldehydes to produce protected hydrazones. In the second step of the procedure, under the action of sodium hydride, the addition of another aldehyde affords non-symmetrical azines in the reaction with the protected hydrazine. The procedure was shown to be a useful and effective method. In this, the second part of our study, we present results devoted to the preparation and full identification of non-symmetrical azines.
  • This paper deals with the preparation of a variously substituted non-symmetrical azine set. The starting molecule for their preparation was a protected hydrazone. The protection was performed applying Zwierzak’s method. This procedure is based on the transfer of hydrazine to diethyl-hydrazidophosphate, which reacts with aldehydes to produce protected hydrazones. In the second step of the procedure, under the action of sodium hydride, the addition of another aldehyde affords non-symmetrical azines in the reaction with the protected hydrazine. The procedure was shown to be a useful and effective method. In this, the second part of our study, we present results devoted to the preparation and full identification of non-symmetrical azines. (en)
Title
  • Substituted homoallenyl aldehydes and their derivatives. Part 2: Azines
  • Substituted homoallenyl aldehydes and their derivatives. Part 2: Azines (en)
skos:prefLabel
  • Substituted homoallenyl aldehydes and their derivatives. Part 2: Azines
  • Substituted homoallenyl aldehydes and their derivatives. Part 2: Azines (en)
skos:notation
  • RIV/00216224:14310/13:00065929!RIV14-GA0-14310___
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  • P(GA203/09/1345)
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  • 1
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  • 108906
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  • RIV/00216224:14310/13:00065929
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  • allenyl; azine; aldehyde; hydrazone; deprotonation; non-symmetrical (en)
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  • PL - Polská republika
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  • [175F6DF8D628]
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  • Chemical Papers
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  • 67
http://linked.open...iv/tvurceVysledku
  • Galeta, Juraj
  • Man, Stanislav
  • Potáček, Milan
  • Valoušková, Aneta
http://linked.open...ain/vavai/riv/wos
  • 000308951200006
issn
  • 0366-6352
number of pages
http://bibframe.org/vocab/doi
  • 10.2478/s11696-012-0238-z
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  • 14310
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