"000324077700057" . "Layered zinc hydroxide sulphate (ZHS) was prepared by microwave-assisted hydrothermal precipitation of zinc sulphate monohydrate with hexamethylenetetramine. Under ambient conditions, the structure of ZHS determined by X-ray diffraction (XRD) was found to be a mixture of zinc hydroxide sulphate pentahydrate and tetrahydrate. Fourier transform infrared (FTIR) spectroscopy was used for characterization of the prepared materials. Based on the interpretation of ZHS's thermal decomposition profile obtained by thermogravimetric analysis, ZnO of high purity was prepared by calcination at 900 C for 2 h. The structure of the resulting ZnO was confirmed by the XRD. The morphology examination by scanning electron microscopy revealed a porous mesh-like ZnO structure developed from the ZHS precursor at the expense of mass removal due to the release of water and sulphate during the calcination." . . "P(ED2.1.00/03.0111), P(EE.2.3.20.0104)" . "77282" . "Hexagonal ZnO porous plates prepared from microwave synthesized layered zinc hydroxide sulphate via thermal decomposition" . . "Pastorek, Miroslav" . "Layered zinc hydroxide sulphate (ZHS) was prepared by microwave-assisted hydrothermal precipitation of zinc sulphate monohydrate with hexamethylenetetramine. Under ambient conditions, the structure of ZHS determined by X-ray diffraction (XRD) was found to be a mixture of zinc hydroxide sulphate pentahydrate and tetrahydrate. Fourier transform infrared (FTIR) spectroscopy was used for characterization of the prepared materials. Based on the interpretation of ZHS's thermal decomposition profile obtained by thermogravimetric analysis, ZnO of high purity was prepared by calcination at 900 C for 2 h. The structure of the resulting ZnO was confirmed by the XRD. The morphology examination by scanning electron microscopy revealed a porous mesh-like ZnO structure developed from the ZHS precursor at the expense of mass removal due to the release of water and sulphate during the calcination."@en . . "Hexagonal ZnO porous plates prepared from microwave synthesized layered zinc hydroxide sulphate via thermal decomposition"@en . "Hexagonal ZnO porous plates prepared from microwave synthesized layered zinc hydroxide sulphate via thermal decomposition" . . "[A7161D1F619D]" . "RIV/70883521:28610/13:43869987!RIV14-MSM-28610___" . "http://www.sciencedirect.com/science/article/pii/S0025540813005151" . "C. X-ray diffraction; C. Thermogravimetric analysis (TGA); C. Infrared spectroscopy; A. Oxides; A. Layered compounds"@en . . "Sedl\u00E1k, Jakub" . "GB - Spojen\u00E9 kr\u00E1lovstv\u00ED Velk\u00E9 Brit\u00E1nie a Severn\u00EDho Irska" . . "10.1016/j.materresbull.2013.06.018" . . . . . "Ku\u0159itka, Ivo" . . "Machovsk\u00FD, Michal" . . "48" . "6"^^ . . "4"^^ . "Materials Research Bulletin: an international journal reporting research on the synthesis, structure, and properties of materials" . "4"^^ . "10" . . . "Hexagonal ZnO porous plates prepared from microwave synthesized layered zinc hydroxide sulphate via thermal decomposition"@en . . . . . "RIV/70883521:28610/13:43869987" . "28610" . . . . "0025-5408" .