"To prepare bicrystals of an Fe-2.5wt% Si alloy with a 36.9?(100) twist grain boundary perpendicular to the rod axis, the floating zone technique was applied. The method is based on growing a single crystal, melting a zone in its center, rotating both unmelted parts by desired angle, and crystallizing slowly the molten zone. During the solidification of the zone, macrosegregation occurs. Its range is studied and described. The differences in chemical composition can be reduced by annealing the bicrystal at temperatures below melting point." . "Growth of alloy bicrystals with twist grain boundaries by the floating zone technique"@en . . "0022-0248" . "e1597;e1602" . "Growth of alloy bicrystals with twist grain boundaries by the floating zone technique" . "522958" . "RIV/68378271:_____/05:00021686" . . . . "To prepare bicrystals of an Fe-2.5wt% Si alloy with a 36.9?(100) twist grain boundary perpendicular to the rod axis, the floating zone technique was applied. The method is based on growing a single crystal, melting a zone in its center, rotating both unmelted parts by desired angle, and crystallizing slowly the molten zone. During the solidification of the zone, macrosegregation occurs. Its range is studied and described. The differences in chemical composition can be reduced by annealing the bicrystal at temperatures below melting point."@en . "NL - Nizozemsko" . . "-" . . "[2D4BEB9D8224]" . "R\u016Fst bikrystal\u016F slitin se zkrutovou hranic\u00ED metodou vysut\u00E9 zon\u00E1ln\u00ED tavby"@cs . . "6"^^ . "Journal of Crystal Growth" . . . . . "3"^^ . . "3"^^ . "La\u0161ek, Ji\u0159\u00ED" . . . "characterization; interfaces; segregation; floating zone technique; metals"@en . . . "RIV/68378271:_____/05:00021686!RIV06-AV0-68378271" . "R\u016Fst bikrystal\u016F slitin se zkrutovou hranic\u00ED metodou vysut\u00E9 zon\u00E1ln\u00ED tavby"@cs . . "Bartu\u0161ka, Pavel" . . . . "Growth of alloy bicrystals with twist grain boundaries by the floating zone technique" . . "P(GA106/02/0253), P(IAA1010414), Z(AV0Z10100520)" . . "Lej\u010Dek, Pavel" . "Metoda visut\u00E9 zon\u00E1ln\u00ED tavby byla pou\u017Eita k p\u0159\u00EDprav\u011B bikrystal\u016F slitiny Fe-2.5hm.% s 36.9?(100)zkrutovou hranic\u00ED. Metoda je zalo\u017Eena na r\u016Fstu monokrystalu, roztaven\u00ED jeho st\u0159edov\u00E9 \u010D\u00E1sti rotace obou neroztaven\u00FDch \u010D\u00E1st\u00ED o po\u017Eadovan\u00FD \u00FAhel a pomal\u00E9 krystalizaci roztaven\u00E9 z\u00F3ny. B\u011Bhem tuhnut\u00ED z\u00F3ny doch\u00E1z\u00ED k makrosegregaci p\u0159\u00EDm\u011Bs\u00ED. Jej\u00ED rozsah je studov\u00E1n a pops\u00E1n. Rozd\u00EDly v chemick\u00E9m slo\u017Een\u00ED lze redukovat \u017E\u00EDh\u00E1n\u00EDm bikrystalu p\u0159i teplot\u00E1ch pod bodem t\u00E1n\u00ED."@cs . "Growth of alloy bicrystals with twist grain boundaries by the floating zone technique"@en . "275" .