. . "The process for preparing titanium silicate Ti-ZSM-5 of the present invention is characterized in that a half-finished product with Si:Ti ratio = 35:1 to 40:1 is prepared by hydrolysis of 150 to 170 parts of a tetraalkoxysilane and tetraalkoxytitanate mixture containing Si and Ti in a ratio in the range of 9:1 to 20:1, at a temperature ranging from 0 to 7 degC by the addition of 320 to 330 parts of a solution of tetrapropylammonium hydroxide and alkali-free silica sol containing 3 to 30 percent by weight of SiOi2. Subsequently, 720 to 770 parts of alkali-free silica sol are added. Then the mixture is dried and treated to a powder half-finished product with particle size at the most 100 microns.; Then, 2 to 5.5 parts of tetrapropylammonium hydroxide, 14 to 15 parts of water and 0.05 to 0.07 parts of titanium silicate Ti-ZSM-5 inoculation crystals are added to 6 parts of the half-finished product. Subsequent synthesis takes place at a temperature ranging from 150 to 170 degC for a period of 1 to 5 days. Finally, the product is subjected to filtration, washing and drying at a temperature ranging from 80 to 120 degC"@en . . "titanium silicate, Ti-ZSM-5, tetrapropylammonium hydroxide"@en . "P\u0159i v\u00FDrob\u011B titanosilik\u00E1tu Ti-ZSM-5 se p\u0159iprav\u00ED polotovar s pom\u011Brem Si:Ti = 35:1 a\u017E 40:1 hydrol\u00FDzou 150 a\u017E 170 d\u00EDl\u016F sm\u011Bsi tetraalkoxysilanu a tetraalkoxytitan\u00E1tu, obsahuj\u00EDc\u00ED Si a Ti v pom\u011Bru 9:1 a\u017E 20:1, p\u0159i teplot\u011B 0 a\u017E 7 \u00B0C p\u0159id\u00E1n\u00EDm 320 a\u017E 330 d\u00EDl\u016F roztoku tetrapropylamoniumhydroxidu a alk\u00E1li\u00ED prost\u00E9ho k\u0159emi\u010Dit\u00E9ho solu s obsahem 3 a\u017E 30 % hmotn. SiO₂. N\u00E1sledn\u011B se p\u0159id\u00E1 720 a\u017E 770 d\u00EDl\u016F alk\u00E1li\u00ED prost\u00E9ho k\u0159emi\u010Dit\u00E9ho solu. Pak se sm\u011Bs vysu\u0161\u00ED a uprav\u00ED na pr\u00E1\u0161kov\u00FD polotovar o velikosti \u010D\u00E1stic nejv\u00FD\u0161e 100 \u00B5m. Pak se k 6 d\u00EDl\u016Fm polotovaru p\u0159id\u00E1 2 a\u017E 5,5 d\u00EDl\u016F tetrapropylamoniumhydroxidu, 14 a\u017E 15 d\u00EDl\u016F vody a 0,05 a\u017E 0,07 d\u00EDl\u016F o\u010Dkovac\u00EDch krystal\u016F titanosilik\u00E1tu Ti-ZSM-5. N\u00E1sledn\u00E1 synt\u00E9za prob\u00EDh\u00E1 p\u0159i teplot\u011B 150 a\u017E 170 \u00B0C po dobu 1 a\u017E 5 dn\u016F. Pak se produkt zfiltruje, promyje a usu\u0161\u00ED p\u0159i teplot\u011B 80 a\u017E 120 \u00B0C."@cs . . . "P(FT-TA3/080)" . "Hol\u00EDkov\u00E1, Stanislava" . . . "Process for preparing titanium silicate Ti-ZSM-5 from half-finished product"@en . . . . . "Zp\u016Fsob v\u00FDroby titanosilik\u00E1tu Ti-ZSM-5 z polotovaru" . "RIV/62243136:_____/11:#0000175" . "RIV/62243136:_____/11:#0000175!RIV12-MPO-62243136" . . "Zp\u016Fsob v\u00FDroby titanosilik\u00E1tu Ti-ZSM-5 z polotovaru"@cs . "Krupov\u00E1, Dagmar" . . . "V\u00FDzkumn\u00FD \u00FAstav anorganick\u00E9 chemie, a.s., \u00DAst\u00ED nad Labem" . "Prague" . "Zp\u016Fsob v\u00FDroby titanosilik\u00E1tu Ti-ZSM-5 z polotovaru" . "Process for preparing titanium silicate Ti-ZSM-5 from half-finished product"@en . "http://spisy.upv.cz/Patents/FullDocuments/302/302444.pdf" . . . . "Tokarov\u00E1, V\u011Bnceslava" . . . "3"^^ . "[3D93869BB6F3]" . . "302444" . . "2011-04-08+02:00"^^ . "Zp\u016Fsob v\u00FDroby titanosilik\u00E1tu Ti-ZSM-5 z polotovaru"@cs . . "3"^^ . . "243680" . "\u00DA\u0159ad pr\u016Fmyslov\u00E9ho vlastnictv\u00ED" . . "P\u0159i v\u00FDrob\u011B titanosilik\u00E1tu Ti-ZSM-5 se p\u0159iprav\u00ED polotovar s pom\u011Brem Si:Ti = 35:1 a\u017E 40:1 hydrol\u00FDzou 150 a\u017E 170 d\u00EDl\u016F sm\u011Bsi tetraalkoxysilanu a tetraalkoxytitan\u00E1tu, obsahuj\u00EDc\u00ED Si a Ti v pom\u011Bru 9:1 a\u017E 20:1, p\u0159i teplot\u011B 0 a\u017E 7 \u00B0C p\u0159id\u00E1n\u00EDm 320 a\u017E 330 d\u00EDl\u016F roztoku tetrapropylamoniumhydroxidu a alk\u00E1li\u00ED prost\u00E9ho k\u0159emi\u010Dit\u00E9ho solu s obsahem 3 a\u017E 30 % hmotn. SiO₂. N\u00E1sledn\u011B se p\u0159id\u00E1 720 a\u017E 770 d\u00EDl\u016F alk\u00E1li\u00ED prost\u00E9ho k\u0159emi\u010Dit\u00E9ho solu. Pak se sm\u011Bs vysu\u0161\u00ED a uprav\u00ED na pr\u00E1\u0161kov\u00FD polotovar o velikosti \u010D\u00E1stic nejv\u00FD\u0161e 100 \u00B5m. Pak se k 6 d\u00EDl\u016Fm polotovaru p\u0159id\u00E1 2 a\u017E 5,5 d\u00EDl\u016F tetrapropylamoniumhydroxidu, 14 a\u017E 15 d\u00EDl\u016F vody a 0,05 a\u017E 0,07 d\u00EDl\u016F o\u010Dkovac\u00EDch krystal\u016F titanosilik\u00E1tu Ti-ZSM-5. N\u00E1sledn\u00E1 synt\u00E9za prob\u00EDh\u00E1 p\u0159i teplot\u011B 150 a\u017E 170 \u00B0C po dobu 1 a\u017E 5 dn\u016F. Pak se produkt zfiltruje, promyje a usu\u0161\u00ED p\u0159i teplot\u011B 80 a\u017E 120 \u00B0C." .