"CZ - \u010Cesk\u00E1 republika" . "25310" . . "Z(MSM 253100002)" . "Byla vyvinuta metoda isotachoforetick\u00E9ho stanoven\u00ED kyseliny thiodiglykolov\u00E9 (TdGA) v\u00A0mo\u010Di zahrnuj\u00EDc\u00ED odsolen\u00ED a \u00FApravu pH analyzovan\u00E9ho vzorku. Soli p\u0159\u00EDtomn\u00E9 v\u00A0mo\u010Di byly vysr\u00E1\u017Eeny p\u0159\u00EDdavkem ethanolu. TdGA byla stanovov\u00E1na v\u00A0anodick\u00E9m izotachoforetick\u00E9m modu v\u00A00,01M HCl s\u00A0obsahem 0,01 % (2-hydrxyethyl)celul\u00F3zy jako vod\u00EDc\u00EDm elektrolytu o pH 4,0 (upraveno kyselinou \u03B5-aminokapronovou). 0,01M kyselina octov\u00E1 slou\u017Eila jako koncov\u00FD elektrolyt. Reprodukovatelnost stanoven\u00ED TdGA byla velice dobr\u00E1, relativn\u00ED sm\u011Brodatn\u00E1 odchylka stanoven\u00ED pro koncentraci 90 mg L-1 byla men\u0161\u00ED ne\u017E 1,5 %."@cs . "580690" . . . . "RIV/00216275:25310/04:00001410" . . "Postup izotachoforetick\u00E9ho stanoven\u00ED kyseliny thiodiglykolov\u00E9 v\u00A0mo\u010Di po odsolen\u00ED a \u00FAprav\u011B pH analyzovan\u00E9ho vzorku"@cs . "Postup izotachoforetick\u00E9ho stanoven\u00ED kyseliny thiodiglykolov\u00E9 v\u00A0mo\u010Di po odsolen\u00ED a \u00FAprav\u011B pH analyzovan\u00E9ho vzorku" . "5" . "[C80414E349EE]" . . . "98" . "4"^^ . "Fadrn\u00E1, Ren\u00E1ta" . "260-263" . "0009-2770" . "Procedure for isotachophoretic determination of thiodiglycolic acid in urine using desalination of the analyzed sample"@en . "Ch\u00FDlkov\u00E1, Jarom\u00EDra" . "Byla vyvinuta metoda isotachoforetick\u00E9ho stanoven\u00ED kyseliny thiodiglykolov\u00E9 (TdGA) v\u00A0mo\u010Di zahrnuj\u00EDc\u00ED odsolen\u00ED a \u00FApravu pH analyzovan\u00E9ho vzorku. Soli p\u0159\u00EDtomn\u00E9 v\u00A0mo\u010Di byly vysr\u00E1\u017Eeny p\u0159\u00EDdavkem ethanolu. TdGA byla stanovov\u00E1na v\u00A0anodick\u00E9m izotachoforetick\u00E9m modu v\u00A00,01M HCl s\u00A0obsahem 0,01 % (2-hydrxyethyl)celul\u00F3zy jako vod\u00EDc\u00EDm elektrolytu o pH 4,0 (upraveno kyselinou \u03B5-aminokapronovou). 0,01M kyselina octov\u00E1 slou\u017Eila jako koncov\u00FD elektrolyt. Reprodukovatelnost stanoven\u00ED TdGA byla velice dobr\u00E1, relativn\u00ED sm\u011Brodatn\u00E1 odchylka stanoven\u00ED pro koncentraci 90 mg L-1 byla men\u0161\u00ED ne\u017E 1,5 %." . . . "A procedure for the isotachophoretic determination of thiodiglycolic acid (TdGA) in urine after desalination and pH adjustment of analyzed sample was elaborated. The salts present in urine were precipitated by addition of ethanol. TdGA was determined in anionic isotachophoretic mode in 0.01M HCl as a leading electrolyte containing 0.01 % (2-hydroxyethyl)cellulose at pH 4.0 (adjusted with \u03B5-aminocaproic acid). 0.01M acetic acid was used as a terminating electrolyte. The reproducibility of TdGA determination was very good, the relative standard deviation was less than 1.5 % for a concentration of TdGA 90 mg L-1."@en . . . "Postup izotachoforetick\u00E9ho stanoven\u00ED kyseliny thiodiglykolov\u00E9 v\u00A0mo\u010Di po odsolen\u00ED a \u00FAprav\u011B pH analyzovan\u00E9ho vzorku" . . "Chemick\u00E9 Listy" . "Postup izotachoforetick\u00E9ho stanoven\u00ED kyseliny thiodiglykolov\u00E9 v\u00A0mo\u010Di po odsolen\u00ED a \u00FAprav\u011B pH analyzovan\u00E9ho vzorku"@cs . "2"^^ . . "RIV/00216275:25310/04:00001410!RIV08-MSM-25310___" . "2"^^ . . "Procedure for isotachophoretic determination of thiodiglycolic acid in urine using desalination of the analyzed sample"@en . . . "thiodiglycolic acid; desalination; isotachophoresis"@en .