. . . "The right sample preparation for thermal analysis can avoid obtaining unreasonable results. Results are influenced by material characteristics, sample pan used, and by cooling and warming rates and temperature range. Selection of appropriate sample size and weight together with sample homogeneity are important preconditions for successful thermal analysis. Sensitivity and resolution of thermal analysis is influenced by sample weight, sample water content and also by sample pan type and cooling/warming rate. Sample pan configuration depends on characteristic of measured material. High sample water content increases sensitivity of thermal analysis but for exact measurement the use of hermetic pans is necessary to avoid loss of sample mass." . "978-80-87011-05-8" . "DSC sample preparation"@en . "RIV/00027006:_____/07:2196" . . "Faltus, Milo\u0161" . "Spr\u00E1vn\u00E1 p\u0159\u00EDprava vzorku pro termickou anal\u00FDzu m\u016F\u017Ee zabr\u00E1nit z\u00EDsk\u00E1n\u00ED nep\u0159esn\u00FDch v\u00FDsledk\u016F. V\u00FDsledky jsou ovlivn\u011Bny vlastnostmi m\u011B\u0159en\u00E9ho materi\u00E1lu, pou\u017Eit\u00FDmi m\u011B\u0159\u00EDc\u00EDmi p\u00E1nvi\u010Dkami, rychlost\u00ED chlazen\u00ED \u010Di oh\u0159evu a teplotn\u00EDm rozsahem m\u011B\u0159en\u00ED. V\u00FDb\u011Br vhodn\u00E9 velikosti a hmotnosti vzorku spolu s homogenitou vzorku jsou d\u016Fle\u017Eit\u00FDm p\u0159edpokladem pro \u00FAsp\u011B\u0161nou termickou anal\u00FDzu. Citlivost a rozli\u0161en\u00ED termick\u00E9 anal\u00FDzy jsou ovlivn\u011Bny velikost\u00ED vzorku, obsahem vody ve vzorku a tak\u00E9 typem m\u011B\u0159\u00EDc\u00ED p\u00E1nvi\u010Dky a rychlost\u00ED chlazen\u00ED a oh\u0159evu. V\u00FDb\u011Br vhodn\u00E9ho typu p\u00E1nvi\u010Dky z\u00E1le\u017E\u00ED na vlastnostech m\u011B\u0159en\u00E9ho materi\u00E1lu. Vysok\u00FD obsah vody ve vzorku zvy\u0161uje citlivost termick\u00E9 anal\u00FDzy, ale z\u00E1rove\u0148 je nezbytn\u00E9 pou\u017E\u00EDt pro m\u011B\u0159en\u00ED hermeticky uzav\u00EDrateln\u00E9 p\u00E1nvi\u010Dky pro zabr\u00E1n\u011Bn\u00ED ztr\u00E1ty \u010D\u00E1sti hmoty vzorku."@cs . "Methods of Thermal Analysis in Plant Cryopreservation" . . . . "DSC sample preparation" . "P(QF3039), Z(MZE0002700602)" . "P\u0159\u00EDprava vzork\u016F pro DSC"@cs . . "DSC sample preparation"@en . "Praha" . . . . "DSC; differencial scanning calorimetry; sample size; pan; cooling rate"@en . . "1"^^ . "[C773B889E55D]" . . . . . . . "418209" . . "1"^^ . "V\u00FDzkumn\u00FD \u00FAstav rostlinn\u00E9 v\u00FDroby, v.v.i., Praha" . "54;59" . "RIV/00027006:_____/07:2196!RIV08-MZE-00027006" . . "V\u00FDzkumn\u00FD \u00FAstav rostlinn\u00E9 v\u00FDroby,v.v.i." . "6"^^ . "DSC sample preparation" . "2007-09-17+02:00"^^ . "The right sample preparation for thermal analysis can avoid obtaining unreasonable results. Results are influenced by material characteristics, sample pan used, and by cooling and warming rates and temperature range. Selection of appropriate sample size and weight together with sample homogeneity are important preconditions for successful thermal analysis. Sensitivity and resolution of thermal analysis is influenced by sample weight, sample water content and also by sample pan type and cooling/warming rate. Sample pan configuration depends on characteristic of measured material. High sample water content increases sensitivity of thermal analysis but for exact measurement the use of hermetic pans is necessary to avoid loss of sample mass."@en . "P\u0159\u00EDprava vzork\u016F pro DSC"@cs .