"68" . . "\u0160tengl, V\u00E1clav" . "Hou\u0161kov\u00E1, Vendula" . . "0022-3697" . "436124" . . "\u010Cl\u00E1nek popisuje p\u0159\u00EDpravu a charakterizaci nano\u010D\u00E1stic oxidu zine\u010Dnat\u00E9ho (ZnO). Nanostrukturn\u00ED ZnO byl p\u0159ipraven ze sulfidu zine\u010Dnat\u00E9ho (ZnS). Nano\u010D\u00E1stice ZnS byly p\u0159ipraveny homogenn\u00ED hydrol\u00FDzou s\u00EDranu zine\u010Dnat\u00E9ho za p\u0159\u00EDtomnosti thioacetamidu p\u0159i 80 \u00B0C. \u017D\u00EDh\u00E1n\u00EDm v kysl\u00EDkov\u00E9 atmosf\u00E9\u0159e p\u0159i 400 \u00B0C byl z\u00EDsk\u00E1n ZnO. Jak ZnS, tak i ZnO prepar\u00E1ty byly charakterizov\u00E1ny rtg. difrak\u010Dn\u00ED anal\u00FDzou (XRD), \u0159\u00E1dkovac\u00EDm elektronov\u00FDm mikroskopem (SEM) a transmisn\u00EDm elektronov\u00FDm mikroskopem s vysokou rozli\u0161ovac\u00ED schopnost\u00ED (HRTEM), d\u00E1le technikou m\u011B\u0159en\u00ED elektronov\u00E9 difrakce (SAED), m\u011B\u0159en\u00EDm specifick\u00E9ho povrchu (BET) a porozity (BHJ). Fotokatalytick\u00E1 aktivita takto p\u0159ipraven\u00FDch vzork\u016F byla m\u011B\u0159ena p\u0159i rozkladu barviva Oran\u017E II ve vodn\u00E9m prost\u0159ed\u00ED p\u0159i osvitu UV v\u00FDbojkou (365 nm)."@cs . . "Journal of Physics and Chemistry of Solids" . "Photocatalysis; Homogeneous hydrolysis; Zinc oxide"@en . "Nanostructure materials for destruction of warfare agents and eco-toxins prepared by homogeneous hydrolysis with thioacetamide: Part 1\u2014zinc oxide"@en . . "RIV/00000493:G41__/07:#0000259" . . "Oplu\u0161til, Franti\u0161ek" . "Nanostrukturn\u00ED materi\u00E1ly pro destrukci bojov\u00FDch chemick\u00FDch l\u00E1tek a eko-toxin\u016F p\u0159ipraven\u00E9 homogenn\u00ED hydrol\u00FDzou pomoc\u00ED thioacetamidu: \u010C\u00E1st 1 - Oxid zinku"@cs . "Bakardjieva, Snejana" . . "Nanostructure materials for destruction of warfare agents and eco-toxins prepared by homogeneous hydrolysis with thioacetamide: Part 1\u2014zinc oxide" . "6"^^ . "G41" . "Nanostrukturn\u00ED materi\u00E1ly pro destrukci bojov\u00FDch chemick\u00FDch l\u00E1tek a eko-toxin\u016F p\u0159ipraven\u00E9 homogenn\u00ED hydrol\u00FDzou pomoc\u00ED thioacetamidu: \u010C\u00E1st 1 - Oxid zinku"@cs . "RIV/00000493:G41__/07:#0000259!RIV09-MO0-G41_____" . . "5-6" . "5"^^ . . "Kalendov\u00E1, Andrea" . . . "Nanostructure materials for destruction of warfare agents and eco-toxins prepared by homogeneous hydrolysis with thioacetamide: Part 1\u2014zinc oxide"@en . . "P(OSVTUO2006010), Z(AV0Z40320502)" . "US - Spojen\u00E9 st\u00E1ty americk\u00E9" . "1"^^ . . "Murafa, Natalyia" . . "Nanostructure materials for destruction of warfare agents and eco-toxins prepared by homogeneous hydrolysis with thioacetamide: Part 1\u2014zinc oxide" . "[B0CD9C516FAD]" . . "Preparation method and characterizastion of the zink oxide (ZnO) nanoparticles are described in the article. Nanoparticles of ZnO were acquired from zinc sulphide (ZnS) nanoparticles. The ZnS nanoparticles were prepared by homogeneous hydrolysis of zinc sulphate and thioacetamide (TAA) at 80 \u00B0C. After annealing at temperature above 400 \u00B0C in oxygen atmosphere, zinc oxide (ZnO) nanoparticles were obtained. The ZnS and ZnO nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), high resolution transmission microscopy (HRTEM), selected area electron diffraction (SAED), by BET and BJH methods used for surface area and porosity determination. The photocatalytic activity of the as-prepared ZnO samples was determined by the decomposition of Orange II in the aqueous solution under UV irradiation of 365 nm of wavelength."@en . . . "Preparation method and characterizastion of the zink oxide (ZnO) nanoparticles are described in the article. Nanoparticles of ZnO were acquired from zinc sulphide (ZnS) nanoparticles. The ZnS nanoparticles were prepared by homogeneous hydrolysis of zinc sulphate and thioacetamide (TAA) at 80 \u00B0C. After annealing at temperature above 400 \u00B0C in oxygen atmosphere, zinc oxide (ZnO) nanoparticles were obtained. The ZnS and ZnO nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), high resolution transmission microscopy (HRTEM), selected area electron diffraction (SAED), by BET and BJH methods used for surface area and porosity determination. The photocatalytic activity of the as-prepared ZnO samples was determined by the decomposition of Orange II in the aqueous solution under UV irradiation of 365 nm of wavelength." .