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Statements

Subject Item
n2:RIV%2F70883521%3A28610%2F13%3A43869987%21RIV14-MSM-28610___
rdf:type
skos:Concept n15:Vysledek
rdfs:seeAlso
http://www.sciencedirect.com/science/article/pii/S0025540813005151
dcterms:description
Layered zinc hydroxide sulphate (ZHS) was prepared by microwave-assisted hydrothermal precipitation of zinc sulphate monohydrate with hexamethylenetetramine. Under ambient conditions, the structure of ZHS determined by X-ray diffraction (XRD) was found to be a mixture of zinc hydroxide sulphate pentahydrate and tetrahydrate. Fourier transform infrared (FTIR) spectroscopy was used for characterization of the prepared materials. Based on the interpretation of ZHS's thermal decomposition profile obtained by thermogravimetric analysis, ZnO of high purity was prepared by calcination at 900 C for 2 h. The structure of the resulting ZnO was confirmed by the XRD. The morphology examination by scanning electron microscopy revealed a porous mesh-like ZnO structure developed from the ZHS precursor at the expense of mass removal due to the release of water and sulphate during the calcination. Layered zinc hydroxide sulphate (ZHS) was prepared by microwave-assisted hydrothermal precipitation of zinc sulphate monohydrate with hexamethylenetetramine. Under ambient conditions, the structure of ZHS determined by X-ray diffraction (XRD) was found to be a mixture of zinc hydroxide sulphate pentahydrate and tetrahydrate. Fourier transform infrared (FTIR) spectroscopy was used for characterization of the prepared materials. Based on the interpretation of ZHS's thermal decomposition profile obtained by thermogravimetric analysis, ZnO of high purity was prepared by calcination at 900 C for 2 h. The structure of the resulting ZnO was confirmed by the XRD. The morphology examination by scanning electron microscopy revealed a porous mesh-like ZnO structure developed from the ZHS precursor at the expense of mass removal due to the release of water and sulphate during the calcination.
dcterms:title
Hexagonal ZnO porous plates prepared from microwave synthesized layered zinc hydroxide sulphate via thermal decomposition Hexagonal ZnO porous plates prepared from microwave synthesized layered zinc hydroxide sulphate via thermal decomposition
skos:prefLabel
Hexagonal ZnO porous plates prepared from microwave synthesized layered zinc hydroxide sulphate via thermal decomposition Hexagonal ZnO porous plates prepared from microwave synthesized layered zinc hydroxide sulphate via thermal decomposition
skos:notation
RIV/70883521:28610/13:43869987!RIV14-MSM-28610___
n15:predkladatel
n21:orjk%3A28610
n3:aktivita
n16:P
n3:aktivity
P(ED2.1.00/03.0111), P(EE.2.3.20.0104)
n3:cisloPeriodika
10
n3:dodaniDat
n7:2014
n3:domaciTvurceVysledku
n5:4717791 n5:7874138 n5:8125562 n5:9184988
n3:druhVysledku
n12:J
n3:duvernostUdaju
n19:S
n3:entitaPredkladatele
n17:predkladatel
n3:idSjednocenehoVysledku
77282
n3:idVysledku
RIV/70883521:28610/13:43869987
n3:jazykVysledku
n13:eng
n3:klicovaSlova
C. X-ray diffraction; C. Thermogravimetric analysis (TGA); C. Infrared spectroscopy; A. Oxides; A. Layered compounds
n3:klicoveSlovo
n11:C.%20Infrared%20spectroscopy n11:C.%20Thermogravimetric%20analysis%20%28TGA%29 n11:C.%20X-ray%20diffraction n11:A.%20Layered%20compounds n11:A.%20Oxides
n3:kodStatuVydavatele
GB - Spojené království Velké Británie a Severního Irska
n3:kontrolniKodProRIV
[A7161D1F619D]
n3:nazevZdroje
Materials Research Bulletin: an international journal reporting research on the synthesis, structure, and properties of materials
n3:obor
n9:JJ
n3:pocetDomacichTvurcuVysledku
4
n3:pocetTvurcuVysledku
4
n3:projekt
n18:ED2.1.00%2F03.0111 n18:EE.2.3.20.0104
n3:rokUplatneniVysledku
n7:2013
n3:svazekPeriodika
48
n3:tvurceVysledku
Pastorek, Miroslav Sedlák, Jakub Kuřitka, Ivo Machovský, Michal
n3:wos
000324077700057
s:issn
0025-5408
s:numberOfPages
6
n10:doi
10.1016/j.materresbull.2013.06.018
n20:organizacniJednotka
28610