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Statements

Subject Item
n2:RIV%2F70883521%3A28110%2F11%3A43867173%21RIV12-MSM-28110___
rdf:type
skos:Concept n15:Vysledek
dcterms:description
In this paper we present a simple two stage preparation method of nanostructured zinc oxide microparticles by using microwave-assisted solvothermal synthesis. Zinc acetate dihydrate and sodium carbonate were used as starting materials, ethyleneglycol (EG), diethyleneglycol (DEG) and demineralised water were used as solvents and polyethylene glycol (PEG) was used as a surface stabilising agent. Obtained powders show various morphology which is influenced by the time duration of microwave assisted reaction and particularly by selection of suitable solvent. According to their morphology, prepared particles are categorised as needle-like structure, platelet structures and urchins-like structures and other shapes, which demonstrates a great potential of this synthesis route. Prepared materials were characterized by Scanning Electron Microscopy (SEM), X-ray diffraction (XRD) and Ultraviolet-visible diffusion reflectance spectroscopy (UV-VIS-DRS). In this paper we present a simple two stage preparation method of nanostructured zinc oxide microparticles by using microwave-assisted solvothermal synthesis. Zinc acetate dihydrate and sodium carbonate were used as starting materials, ethyleneglycol (EG), diethyleneglycol (DEG) and demineralised water were used as solvents and polyethylene glycol (PEG) was used as a surface stabilising agent. Obtained powders show various morphology which is influenced by the time duration of microwave assisted reaction and particularly by selection of suitable solvent. According to their morphology, prepared particles are categorised as needle-like structure, platelet structures and urchins-like structures and other shapes, which demonstrates a great potential of this synthesis route. Prepared materials were characterized by Scanning Electron Microscopy (SEM), X-ray diffraction (XRD) and Ultraviolet-visible diffusion reflectance spectroscopy (UV-VIS-DRS).
dcterms:title
NANOSTRUCTURED ZINC OXIDE MICROPARTICLES WITH VARIOUS MORPHOLOGIES NANOSTRUCTURED ZINC OXIDE MICROPARTICLES WITH VARIOUS MORPHOLOGIES
skos:prefLabel
NANOSTRUCTURED ZINC OXIDE MICROPARTICLES WITH VARIOUS MORPHOLOGIES NANOSTRUCTURED ZINC OXIDE MICROPARTICLES WITH VARIOUS MORPHOLOGIES
skos:notation
RIV/70883521:28110/11:43867173!RIV12-MSM-28110___
n15:predkladatel
n16:orjk%3A28110
n3:aktivita
n19:S n19:P
n3:aktivity
P(ED2.1.00/03.0111), S
n3:dodaniDat
n10:2012
n3:domaciTvurceVysledku
n7:8125562 n7:7874138 n7:9510087 n7:6730604 n7:9184988 n7:4717791
n3:druhVysledku
n21:D
n3:duvernostUdaju
n14:S
n3:entitaPredkladatele
n8:predkladatel
n3:idSjednocenehoVysledku
214802
n3:idVysledku
RIV/70883521:28110/11:43867173
n3:jazykVysledku
n22:eng
n3:klicovaSlova
Nanoparticles; Microparticles; ZnO; Microwave Synthesis
n3:klicoveSlovo
n9:Nanoparticles n9:Microparticles n9:ZnO n9:Microwave%20Synthesis
n3:kontrolniKodProRIV
[83B5BE6A820D]
n3:mistoKonaniAkce
Brno
n3:mistoVydani
Ostrava
n3:nazevZdroje
Nanocon 2011 - sborník příspěvků
n3:obor
n4:CD
n3:pocetDomacichTvurcuVysledku
6
n3:pocetTvurcuVysledku
6
n3:projekt
n6:ED2.1.00%2F03.0111
n3:rokUplatneniVysledku
n10:2011
n3:tvurceVysledku
Kuřitka, Ivo Machovský, Michal Kožáková, Zuzana Pastorek, Miroslav Bažant, Pavel Sedlák, Jakub
n3:typAkce
n18:WRD
n3:zahajeniAkce
2011-09-21+02:00
s:numberOfPages
5
n13:hasPublisher
Tanger spol. s r. o.
n5:isbn
978-80-87294-23-9
n20:organizacniJednotka
28110