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Statements

Subject Item
n2:RIV%2F70565813%3A_____%2F12%3A%230000288%21RIV13-MV0-70565813
rdf:type
skos:Concept n15:Vysledek
dcterms:description
A water-soluble C60 fullerene Derivative (DF) was obtained by reaction of C60 fullerene with peracetic acid and subsequent hydrolysis.The DF water-solution of the concentration of 147 +-0,1 mg/L at ambient temperature and neutral pH remains stable for a long time without the mechanical action (settling) and coagulation of particles. The concentration and the sice of nanoparticles i DFwarer solution were analysed by the NanoSight KM10HSB. Even this system contained a larger particles an analysis after filtration by 0,1 um filter and under 20 x and 10 x objective showed a nice and quite monodispersed distribution of modal particle size 42+53 and 60 nm in concentration 3,5 x 10-8 particles/mL respectively.Comparison of pristine C60 and DF by transmission electron microscopy TEM (100kV) and scannig election microscopy SEMresults showed differences in the size of the irregular complexes and in their crystallinity. Fourier transformed infrared (FTIR) spcterometry of DF detected -OH groups, also C-O and COOH groups. We found this DF solution suitable for subsequent bioeperient in vivo and in vitro due to its hydrophylic properties and relatively homogenous distribution of nanoparticles in aggregates smaller than 60nm. A water-soluble C60 fullerene Derivative (DF) was obtained by reaction of C60 fullerene with peracetic acid and subsequent hydrolysis.The DF water-solution of the concentration of 147 +-0,1 mg/L at ambient temperature and neutral pH remains stable for a long time without the mechanical action (settling) and coagulation of particles. The concentration and the sice of nanoparticles i DFwarer solution were analysed by the NanoSight KM10HSB. Even this system contained a larger particles an analysis after filtration by 0,1 um filter and under 20 x and 10 x objective showed a nice and quite monodispersed distribution of modal particle size 42+53 and 60 nm in concentration 3,5 x 10-8 particles/mL respectively.Comparison of pristine C60 and DF by transmission electron microscopy TEM (100kV) and scannig election microscopy SEMresults showed differences in the size of the irregular complexes and in their crystallinity. Fourier transformed infrared (FTIR) spcterometry of DF detected -OH groups, also C-O and COOH groups. We found this DF solution suitable for subsequent bioeperient in vivo and in vitro due to its hydrophylic properties and relatively homogenous distribution of nanoparticles in aggregates smaller than 60nm.
dcterms:title
Preparation of Water-Soluble Fullerene Derivative by Reaction with Peracetic Acid and Its nanoparticles Size Distribution Preparation of Water-Soluble Fullerene Derivative by Reaction with Peracetic Acid and Its nanoparticles Size Distribution
skos:prefLabel
Preparation of Water-Soluble Fullerene Derivative by Reaction with Peracetic Acid and Its nanoparticles Size Distribution Preparation of Water-Soluble Fullerene Derivative by Reaction with Peracetic Acid and Its nanoparticles Size Distribution
skos:notation
RIV/70565813:_____/12:#0000288!RIV13-MV0-70565813
n15:predkladatel
n16:ico%3A70565813
n3:aktivita
n8:P
n3:aktivity
P(VG20102014049)
n3:cisloPeriodika
1
n3:dodaniDat
n7:2013
n3:domaciTvurceVysledku
n13:1571699
n3:druhVysledku
n11:J
n3:duvernostUdaju
n17:S
n3:entitaPredkladatele
n18:predkladatel
n3:idSjednocenehoVysledku
161373
n3:idVysledku
RIV/70565813:_____/12:#0000288
n3:jazykVysledku
n12:eng
n3:klicovaSlova
Fullerene derivative, NanoSight, electron microsopy (TEM,SEM), Fourier transformed infrared spectrometry (FTIR)
n3:klicoveSlovo
n5:electron%20microsopy%20%28TEM n5:SEM%29 n5:Fullerene%20derivative n5:Fourier%20transformed%20infrared%20spectrometry%20%28FTIR%29 n5:NanoSight
n3:kodStatuVydavatele
US - Spojené státy americké
n3:kontrolniKodProRIV
[572C2245677B]
n3:nazevZdroje
Journal of Materials Science and Engineering A
n3:obor
n14:CB
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
2
n3:projekt
n9:VG20102014049
n3:rokUplatneniVysledku
n7:2012
n3:svazekPeriodika
2
n3:tvurceVysledku
Zemanová, Eva Klouda, Karel
s:issn
2161-6213
s:numberOfPages
12