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Statements

Subject Item
n2:RIV%2F68407700%3A21340%2F03%3A04092405%21RIV%2F2004%2FGA0%2F213404%2FN
rdf:type
skos:Concept n19:Vysledek
dcterms:description
Methylium or ethylium (organic cations) create chemisorbed, but covalently bonded alkoxy species in zeolitic structures. Neutron powder diffraction patterns were collected from evacuated ampoules with samples at room and 7 K on the KSN-2 diffractometer which is placed at the LVR-15 research reactor in Řež near Prague. 13C MAS NMR measurents make possible to distinquish between signals of bridging and terminal methoxy groups. The complete structural parameters (including chemisorbed ions at O1 and O4 in NaX and at O1 in NaY) were determined by Rietveld analysis using GSAS package. Redistribution of Na+ cations in the lattice of both structures after chemisorption was detected Methylium or ethylium (organic cations) create chemisorbed, but covalently bonded alkoxy species in zeolitic structures. Neutron powder diffraction patterns were collected from evacuated ampoules with samples at room and 7 K on the KSN-2 diffractometer which is placed at the LVR-15 research reactor in Řež near Prague. 13C MAS NMR measurents make possible to distinquish between signals of bridging and terminal methoxy groups. The complete structural parameters (including chemisorbed ions at O1 and O4 in NaX and at O1 in NaY) were determined by Rietveld analysis using GSAS package. Redistribution of Na+ cations in the lattice of both structures after chemisorption was detected
dcterms:title
Structural Parameters of Zeolitic Catalysts with Chemisorbed Methyl Groups by Neutron Diffraction and 13C MAS NMR Structural Parameters of Zeolitic Catalysts with Chemisorbed Methyl Groups by Neutron Diffraction and 13C MAS NMR
skos:prefLabel
Structural Parameters of Zeolitic Catalysts with Chemisorbed Methyl Groups by Neutron Diffraction and 13C MAS NMR Structural Parameters of Zeolitic Catalysts with Chemisorbed Methyl Groups by Neutron Diffraction and 13C MAS NMR
skos:notation
RIV/68407700:21340/03:04092405!RIV/2004/GA0/213404/N
n4:strany
111 ; 111
n4:aktivita
n9:P n9:Z
n4:aktivity
P(GA202/03/0891), Z(MSM 210000021)
n4:dodaniDat
n7:2004
n4:domaciTvurceVysledku
n14:5626293 n14:4241312
n4:druhVysledku
n20:D
n4:duvernostUdaju
n10:S
n4:entitaPredkladatele
n11:predkladatel
n4:idSjednocenehoVysledku
629211
n4:idVysledku
RIV/68407700:21340/03:04092405
n4:jazykVysledku
n17:eng
n4:klicovaSlova
zeolites,chemisorbed methyl groups,neutron diffraction
n4:klicoveSlovo
n15:neutron%20diffraction n15:zeolites n15:chemisorbed%20methyl%20groups
n4:kontrolniKodProRIV
[FC523B4050C8]
n4:mistoKonaniAkce
Montpellier
n4:mistoVydani
Villigen
n4:nazevZdroje
Abstract Book of the 3rd European Conference on Neutron Scattering
n4:obor
n6:BM
n4:pocetDomacichTvurcuVysledku
2
n4:pocetTvurcuVysledku
3
n4:projekt
n18:GA202%2F03%2F0891
n4:rokUplatneniVysledku
n7:2003
n4:tvurceVysledku
Bosáček, V. Dlouhá, Maja Vratislav, Stanislav
n4:typAkce
n16:WRD
n4:zahajeniAkce
2003-03-03+01:00
n4:zamer
n12:MSM%20210000021
s:numberOfPages
1
n13:hasPublisher
European Neutron Scattering
n21:organizacniJednotka
21340