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Statements

Subject Item
n2:RIV%2F68378271%3A_____%2F14%3A00434839%21RIV15-AV0-68378271
rdf:type
n3:Vysledek skos:Concept
dcterms:description
A new oxidovanadium(IV) Schiff base complex, VOL2 (1), containing furfuryl pendant group was synthesized by the reaction of the related bidentate O,N-type Schiff base ligand and VO(acac)2. The Schiff base ligand and its vanadyl complex were characterized by 1H-NMR and FT-IR spectra and elemental analysis. The crystal structure of 1 was also determined the single-crystal X-ray analysis. The catalytic activity of the vanadyl Schiff base complex was elucidated in the epoxidation of cyclooctene as a model substrate. In addition, the vanadyl Schiff base complex (1) was thermally decomposed in air at 6 60 deg C and the XRD pattern of the obtained solid showed the formation of the V2O5 nanoparticles with the average size of 52 nm. A new oxidovanadium(IV) Schiff base complex, VOL2 (1), containing furfuryl pendant group was synthesized by the reaction of the related bidentate O,N-type Schiff base ligand and VO(acac)2. The Schiff base ligand and its vanadyl complex were characterized by 1H-NMR and FT-IR spectra and elemental analysis. The crystal structure of 1 was also determined the single-crystal X-ray analysis. The catalytic activity of the vanadyl Schiff base complex was elucidated in the epoxidation of cyclooctene as a model substrate. In addition, the vanadyl Schiff base complex (1) was thermally decomposed in air at 6 60 deg C and the XRD pattern of the obtained solid showed the formation of the V2O5 nanoparticles with the average size of 52 nm.
dcterms:title
Synthesis, characterization, crystal structure determination, catalytic activity and thermal study of a new oxidovanadium(IV) Schiff base complex: production of V2O5 nano-particles Synthesis, characterization, crystal structure determination, catalytic activity and thermal study of a new oxidovanadium(IV) Schiff base complex: production of V2O5 nano-particles
skos:prefLabel
Synthesis, characterization, crystal structure determination, catalytic activity and thermal study of a new oxidovanadium(IV) Schiff base complex: production of V2O5 nano-particles Synthesis, characterization, crystal structure determination, catalytic activity and thermal study of a new oxidovanadium(IV) Schiff base complex: production of V2O5 nano-particles
skos:notation
RIV/68378271:_____/14:00434839!RIV15-AV0-68378271
n4:aktivita
n16:I
n4:aktivity
I
n4:cisloPeriodika
4
n4:dodaniDat
n13:2015
n4:domaciTvurceVysledku
n9:8772274 n9:5796350
n4:druhVysledku
n14:J
n4:duvernostUdaju
n11:S
n4:entitaPredkladatele
n12:predkladatel
n4:idSjednocenehoVysledku
49008
n4:idVysledku
RIV/68378271:_____/14:00434839
n4:jazykVysledku
n17:eng
n4:klicovaSlova
uranium complex; isothiosemicarbazone; crystallography; spectra; thermal stability
n4:klicoveSlovo
n5:crystallography n5:thermal%20stability n5:uranium%20complex n5:isothiosemicarbazone n5:spectra
n4:kodStatuVydavatele
IR - Íránská islámská republika
n4:kontrolniKodProRIV
[BCB00D80747A]
n4:nazevZdroje
Journal of the Iranian Chemical Society
n4:obor
n15:BM
n4:pocetDomacichTvurcuVysledku
2
n4:pocetTvurcuVysledku
6
n4:rokUplatneniVysledku
n13:2014
n4:svazekPeriodika
11
n4:tvurceVysledku
Dušek, Michal Fejfarová, Karla Delkosh, S. Tahmasebi, V. Khalaji, A. D. Grivani, G.
n4:wos
000337597000002
s:issn
1735-207X
s:numberOfPages
10
n10:doi
10.1007/s13738-013-0361-y