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Statements

Subject Item
n2:RIV%2F68378271%3A_____%2F13%3A00425058%21RIV14-AV0-68378271
rdf:type
skos:Concept n13:Vysledek
dcterms:description
Crystals of 2-chloro-benzo-1,3,2-dithiarsole have a strongly modulated structure that can be solved and refined with relative ease in a P1, Z0 = 17 approximate supercell but that is better described as incommensurate. Two conventional refinements (different superstructure approximations that differ in the placement of their crystallographic inversion centers) and a (3 + 1)-dimensional superspace refinement are all nearly equally successful, at least as measured by the usual agreement factors; the data integration, however, shows that the incommensurate description is preferable. Crystals of 2-chloro-benzo-1,3,2-dithiarsole have a strongly modulated structure that can be solved and refined with relative ease in a P1, Z0 = 17 approximate supercell but that is better described as incommensurate. Two conventional refinements (different superstructure approximations that differ in the placement of their crystallographic inversion centers) and a (3 + 1)-dimensional superspace refinement are all nearly equally successful, at least as measured by the usual agreement factors; the data integration, however, shows that the incommensurate description is preferable.
dcterms:title
C6H4S2AsCl: description and interpretation of an incommensurately modulated molecular crystal structure C6H4S2AsCl: description and interpretation of an incommensurately modulated molecular crystal structure
skos:prefLabel
C6H4S2AsCl: description and interpretation of an incommensurately modulated molecular crystal structure C6H4S2AsCl: description and interpretation of an incommensurately modulated molecular crystal structure
skos:notation
RIV/68378271:_____/13:00425058!RIV14-AV0-68378271
n13:predkladatel
n14:ico%3A68378271
n3:aktivita
n5:I
n3:aktivity
I
n3:cisloPeriodika
5
n3:dodaniDat
n17:2014
n3:domaciTvurceVysledku
n6:6297102
n3:druhVysledku
n8:J
n3:duvernostUdaju
n12:S
n3:entitaPredkladatele
n15:predkladatel
n3:idSjednocenehoVysledku
67811
n3:idVysledku
RIV/68378271:_____/13:00425058
n3:jazykVysledku
n18:eng
n3:klicovaSlova
crystal structure analysis; modulated structures; refinement
n3:klicoveSlovo
n11:modulated%20structures n11:refinement n11:crystal%20structure%20analysis
n3:kodStatuVydavatele
DK - Dánské království
n3:kontrolniKodProRIV
[97965A3B4C78]
n3:nazevZdroje
Acta Crystallographica section B - Structural Science
n3:obor
n10:BM
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
5
n3:rokUplatneniVysledku
n17:2013
n3:svazekPeriodika
69
n3:tvurceVysledku
Petříček, Václav Bakus, R. C. Parkin, S. Brock, C. P. Atwood, D. A.
n3:wos
000324881800010
s:issn
0108-7681
s:numberOfPages
13
n16:doi
10.1107/S205251921301782X