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Statements

Subject Item
n2:RIV%2F68081723%3A_____%2F12%3A00385504%21RIV13-AV0-68081723
rdf:type
n11:Vysledek skos:Concept
dcterms:description
DSC and thermomagnetic measurements of Fe75Ni2Si8B13C2 amorphous alloy investigated in 298e973 K temperature range show that alloy remains amorphous up to around 773 K. As thermomagnetic measurements provided more complete information, the alloy ribbon was successively annealed at temperatures chosen on the basis of these measurements and its microstructure was investigated after each annealing cycle using X-ray diffraction and SEM. Two stable, a-Fe(Si) and Fe2B, and one metastable, Fe3B, crystalline phases were identified after annealing. Microstructural analysis showed that Fe3B probably acts as an intermediate in the formation of Fe2B, which formed later than the other two phases. Si and B in the alloy show a tendency to separate into different phases. Analysis of microstructure, combined with chemical composition, showed that after the final annealing at 973 K, alloy ribbon is composed of interdispersed nanocrystals of alpha-Fe(Si) and Fe2B less than 90 nm in size, with no observable larger domains of either phase. DSC and thermomagnetic measurements of Fe75Ni2Si8B13C2 amorphous alloy investigated in 298e973 K temperature range show that alloy remains amorphous up to around 773 K. As thermomagnetic measurements provided more complete information, the alloy ribbon was successively annealed at temperatures chosen on the basis of these measurements and its microstructure was investigated after each annealing cycle using X-ray diffraction and SEM. Two stable, a-Fe(Si) and Fe2B, and one metastable, Fe3B, crystalline phases were identified after annealing. Microstructural analysis showed that Fe3B probably acts as an intermediate in the formation of Fe2B, which formed later than the other two phases. Si and B in the alloy show a tendency to separate into different phases. Analysis of microstructure, combined with chemical composition, showed that after the final annealing at 973 K, alloy ribbon is composed of interdispersed nanocrystals of alpha-Fe(Si) and Fe2B less than 90 nm in size, with no observable larger domains of either phase.
dcterms:title
Influence of thermal treatment on microstructure of Fe75Ni2Si8B13C2 amorphous alloy Influence of thermal treatment on microstructure of Fe75Ni2Si8B13C2 amorphous alloy
skos:prefLabel
Influence of thermal treatment on microstructure of Fe75Ni2Si8B13C2 amorphous alloy Influence of thermal treatment on microstructure of Fe75Ni2Si8B13C2 amorphous alloy
skos:notation
RIV/68081723:_____/12:00385504!RIV13-AV0-68081723
n11:predkladatel
n19:ico%3A68081723
n3:aktivita
n15:P n15:I
n3:aktivity
I, P(1M0512)
n3:cisloPeriodika
1
n3:dodaniDat
n17:2013
n3:domaciTvurceVysledku
n4:7435312 n4:4343883 n4:3246523
n3:druhVysledku
n16:J
n3:duvernostUdaju
n13:S
n3:entitaPredkladatele
n18:predkladatel
n3:idSjednocenehoVysledku
141665
n3:idVysledku
RIV/68081723:_____/12:00385504
n3:jazykVysledku
n6:eng
n3:klicovaSlova
Glasses, metallic; Microstructure; Diffraction; Microscopy
n3:klicoveSlovo
n7:Glasses n7:Microscopy n7:Microstructure n7:metallic n7:Diffraction
n3:kodStatuVydavatele
GB - Spojené království Velké Británie a Severního Irska
n3:kontrolniKodProRIV
[90D3A92E6463]
n3:nazevZdroje
Intermetallics
n3:obor
n14:BM
n3:pocetDomacichTvurcuVysledku
3
n3:pocetTvurcuVysledku
6
n3:projekt
n12:1M0512
n3:rokUplatneniVysledku
n17:2012
n3:svazekPeriodika
25
n3:tvurceVysledku
David, Bohumil Minić, Dušan M. Pizúrová, Naděžda Žák, Tomáš Blagojević, V. Minić, Dragica M.
n3:wos
000303905600012
s:issn
0966-9795
s:numberOfPages
5
n10:doi
10.1016/j.intermet.2012.02.016