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Statements

Subject Item
n2:RIV%2F68081715%3A_____%2F04%3A00102299%21RIV%2F2005%2FGA0%2FA25005%2FN
rdf:type
skos:Concept n16:Vysledek
dcterms:description
For the determination of iodide in urine, a fast, simple and sensitive method of capillary zone electrophoresis was elaborated and tested also for additional complex matrices such as human serum, cooking salt, and seawater. Several approaches were examined for the separation of iodide from other macro- and microcomponents in the tested matrices, and the best results were obtained when host-guest interaction with a-cyclodextrin or ion-pairing with polyethylenimine was employed. In both cases comparable resolution and sensitivity were reached. Due to the relatively high price of cyclodextrin only the method with polyethylenimine was futher optimized and a simple procedure enabling the determination of iodide in untreated human urine, serum cooking salt, and seawater was elaborated Byla vypracována rychlá, jednoduchá a citlivá metoda stanovení jodidu v moči pomocí kapilární zónové elekroforézy. Metoda byla dále testována pro stanovení jodidu ve složitých matricích - lidské sérum, kuchyňská sůl a mořská voda. Byly zkoumány různé přístupy k oddělení jodidu od ostatních makro- a mikrokomponent ve zkoumaných matricích. Nejlepší výsledky byly získány při interakci host-guest s cyklodextrinem nebo iontovém párování s polyetyleniminem. V obou případech bylo dosaženo srovnatelného rozlišení a citlivosti. Vzhledem k relativně vysoké ceně cyklodextrinu byla dále optimalizována pouze metoda s polyetyleniminem a byla vypracována jednoduchá procedura umožňující stanovení jodidu v neupravené lidské moči, séru, kuchyňské soli a mořské vodě For the determination of iodide in urine, a fast, simple and sensitive method of capillary zone electrophoresis was elaborated and tested also for additional complex matrices such as human serum, cooking salt, and seawater. Several approaches were examined for the separation of iodide from other macro- and microcomponents in the tested matrices, and the best results were obtained when host-guest interaction with a-cyclodextrin or ion-pairing with polyethylenimine was employed. In both cases comparable resolution and sensitivity were reached. Due to the relatively high price of cyclodextrin only the method with polyethylenimine was futher optimized and a simple procedure enabling the determination of iodide in untreated human urine, serum cooking salt, and seawater was elaborated
dcterms:title
Fast and simple method for determination of iodide in human urine, serum, sea water, and cooking salt by capillary zone electrophoresis Fast and simple method for determination of iodide in human urine, serum, sea water, and cooking salt by capillary zone electrophoresis Rychlá a jednoduchá metoda stanovení jodidu v lidské moči, séru, mořské vodě a kuchyňské soli pomocí kapilární zónové elektroforézy
skos:prefLabel
Fast and simple method for determination of iodide in human urine, serum, sea water, and cooking salt by capillary zone electrophoresis Fast and simple method for determination of iodide in human urine, serum, sea water, and cooking salt by capillary zone electrophoresis Rychlá a jednoduchá metoda stanovení jodidu v lidské moči, séru, mořské vodě a kuchyňské soli pomocí kapilární zónové elektroforézy
skos:notation
RIV/68081715:_____/04:00102299!RIV/2005/GA0/A25005/N
n3:strany
1102;1110
n3:aktivita
n6:Z n6:P
n3:aktivity
P(GA203/01/0401), P(GA203/02/0023), P(IAA4031103), Z(AV0Z4031919)
n3:cisloPeriodika
7-8
n3:dodaniDat
n18:2005
n3:domaciTvurceVysledku
n5:8976570 n5:7911564
n3:druhVysledku
n15:J
n3:duvernostUdaju
n4:S
n3:entitaPredkladatele
n11:predkladatel
n3:idSjednocenehoVysledku
564172
n3:idVysledku
RIV/68081715:_____/04:00102299
n3:jazykVysledku
n14:eng
n3:klicovaSlova
capillary zone electrophoresis;cooking salt;human serum
n3:klicoveSlovo
n12:human%20serum n12:cooking%20salt n12:capillary%20zone%20electrophoresis
n3:kodStatuVydavatele
DE - Spolková republika Německo
n3:kontrolniKodProRIV
[21CC127AA9F3]
n3:nazevZdroje
Electrophoresis
n3:obor
n13:CB
n3:pocetDomacichTvurcuVysledku
2
n3:pocetTvurcuVysledku
2
n3:projekt
n9:GA203%2F02%2F0023 n9:IAA4031103 n9:GA203%2F01%2F0401
n3:rokUplatneniVysledku
n18:2004
n3:svazekPeriodika
25
n3:tvurceVysledku
Pantůčková, Pavla Křivánková, Ludmila
n3:zamer
n17:AV0Z4031919
s:issn
0173-0835
s:numberOfPages
9