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Statements

Subject Item
n2:RIV%2F67985858%3A_____%2F12%3A00383066%21RIV13-AV0-67985858
rdf:type
n14:Vysledek skos:Concept
dcterms:description
Thin transparent TiO2 layers were created on the conductive ITO glass by means of the templated sol-gel technique and by the subsequent calcination at 450° C. The sol-gel method using molecular templating is based on a chemical process utilizing hydrolysis and polycondesation of metal alkoxides in the core of reverse micelles which allows a production of uniform particles in layers. The sol-gel method was chosen by reason of the sol-gel layers electrodes are transparent and possess very stabile surface. For the preparation of the thin sol-gel TiO 2 films, numerous deposition techniques were applied. This contribution is focused on the study of structural and photo-electrochemical properties of the sol-gel nanostructured layers deposited by two various techniques (a dip-coating and an inkjet printing). The sol's viscosity, concentration, solvent volatility, speed of pulling etc. may influence the final structural properties of layers, such as film thickness, nanoparticles size and surface morphology. The surface properties were determined by XRD, Raman, SEM, AFM and UV-Vis analyses. Photo-induced electrochemical properties were measured by potentiodynamic methods in the three-compartment electrochemical cell. This Pyrex cell contained supporting electrolyte (0.1 M Na2SO4) and the TiO2/ITO electrode was used as a working electrode. As an UV source the polychromatic mercury lamp was employed and the wavelength of the incident light was focused by an interference filter on 365 nm. Thin transparent TiO2 layers were created on the conductive ITO glass by means of the templated sol-gel technique and by the subsequent calcination at 450° C. The sol-gel method using molecular templating is based on a chemical process utilizing hydrolysis and polycondesation of metal alkoxides in the core of reverse micelles which allows a production of uniform particles in layers. The sol-gel method was chosen by reason of the sol-gel layers electrodes are transparent and possess very stabile surface. For the preparation of the thin sol-gel TiO 2 films, numerous deposition techniques were applied. This contribution is focused on the study of structural and photo-electrochemical properties of the sol-gel nanostructured layers deposited by two various techniques (a dip-coating and an inkjet printing). The sol's viscosity, concentration, solvent volatility, speed of pulling etc. may influence the final structural properties of layers, such as film thickness, nanoparticles size and surface morphology. The surface properties were determined by XRD, Raman, SEM, AFM and UV-Vis analyses. Photo-induced electrochemical properties were measured by potentiodynamic methods in the three-compartment electrochemical cell. This Pyrex cell contained supporting electrolyte (0.1 M Na2SO4) and the TiO2/ITO electrode was used as a working electrode. As an UV source the polychromatic mercury lamp was employed and the wavelength of the incident light was focused by an interference filter on 365 nm.
dcterms:title
Electrochemical Properties of TiO2 Electrode Prepared by Various Methods Electrochemical Properties of TiO2 Electrode Prepared by Various Methods
skos:prefLabel
Electrochemical Properties of TiO2 Electrode Prepared by Various Methods Electrochemical Properties of TiO2 Electrode Prepared by Various Methods
skos:notation
RIV/67985858:_____/12:00383066!RIV13-AV0-67985858
n14:predkladatel
n15:ico%3A67985858
n3:aktivita
n9:S n9:P n9:I
n3:aktivity
I, P(GP104/09/P165), P(TA01020804), S
n3:cisloPeriodika
SI
n3:dodaniDat
n13:2013
n3:domaciTvurceVysledku
n12:9345531 n12:3910245 n12:1946609 n12:4232712
n3:druhVysledku
n10:J
n3:duvernostUdaju
n16:S
n3:entitaPredkladatele
n17:predkladatel
n3:idSjednocenehoVysledku
133878
n3:idVysledku
RIV/67985858:_____/12:00383066
n3:jazykVysledku
n5:eng
n3:klicovaSlova
titanium dioxide; sol-gel; photoelectrochemistry
n3:klicoveSlovo
n7:titanium%20dioxide n7:photoelectrochemistry n7:sol-gel
n3:kodStatuVydavatele
NL - Nizozemsko
n3:kontrolniKodProRIV
[7ACDF67C930C]
n3:nazevZdroje
Procedia Engineering
n3:obor
n18:CI
n3:pocetDomacichTvurcuVysledku
4
n3:pocetTvurcuVysledku
6
n3:projekt
n4:TA01020804 n4:GP104%2F09%2FP165
n3:rokUplatneniVysledku
n13:2012
n3:svazekPeriodika
42
n3:tvurceVysledku
Dzik, P. Krýsa, Josef Šolcová, Olga Morozová, Magdalena Klusoň, Petr Veselý, M.
s:issn
1877-7058
s:numberOfPages
8
n19:doi
10.1016/j.proeng.2012.07.450