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Statements

Subject Item
n2:RIV%2F67985858%3A_____%2F12%3A00377301%21RIV13-GA0-67985858
rdf:type
n9:Vysledek skos:Concept
dcterms:description
Two types of the bipolar electrochemical microreactor (BEMR) were investigated for methoxylation of 4-methylanisole: A block-type BEMR with a fixed number of parallel electrodes and a filter-press-type BEMR with a variable number of parallel electrodes. On the basis of a numerical parametric study, the current utilization factor eta was presented for the two microreactors as a function of the dimensionless current I* for different system parameters. Conversion and selectivity of the alkoxylation reaction was studied experimentally and the performance of both BEMR was compared. Even though the optimization of the reactor design is still needed particularly with respect to liquid distribution into the individual parallel microchannels, heat management and gas removal, the presented results indicated that the bipolar arrangement of electrochemical microreactors certainly offers a great potential for the intensification of alkoxylation reactions. Two types of the bipolar electrochemical microreactor (BEMR) were investigated for methoxylation of 4-methylanisole: A block-type BEMR with a fixed number of parallel electrodes and a filter-press-type BEMR with a variable number of parallel electrodes. On the basis of a numerical parametric study, the current utilization factor eta was presented for the two microreactors as a function of the dimensionless current I* for different system parameters. Conversion and selectivity of the alkoxylation reaction was studied experimentally and the performance of both BEMR was compared. Even though the optimization of the reactor design is still needed particularly with respect to liquid distribution into the individual parallel microchannels, heat management and gas removal, the presented results indicated that the bipolar arrangement of electrochemical microreactors certainly offers a great potential for the intensification of alkoxylation reactions.
dcterms:title
Electrochemical Microreactor Design for Alkoxylation Reactions—Experiments and Simulations Electrochemical Microreactor Design for Alkoxylation Reactions—Experiments and Simulations
skos:prefLabel
Electrochemical Microreactor Design for Alkoxylation Reactions—Experiments and Simulations Electrochemical Microreactor Design for Alkoxylation Reactions—Experiments and Simulations
skos:notation
RIV/67985858:_____/12:00377301!RIV13-GA0-67985858
n9:predkladatel
n10:ico%3A67985858
n3:aktivita
n11:P n11:V n11:Z
n3:aktivity
P(GA104/09/0880), V, Z(AV0Z40720504)
n3:cisloPeriodika
4
n3:dodaniDat
n8:2013
n3:domaciTvurceVysledku
n4:2464128 n4:8824274 n4:7561997
n3:druhVysledku
n6:J
n3:duvernostUdaju
n17:S
n3:entitaPredkladatele
n18:predkladatel
n3:idSjednocenehoVysledku
133874
n3:idVysledku
RIV/67985858:_____/12:00377301
n3:jazykVysledku
n7:eng
n3:klicovaSlova
interdigitated band electrodes; high-conversion reactor; water electrolysis
n3:klicoveSlovo
n12:interdigitated%20band%20electrodes n12:high-conversion%20reactor n12:water%20electrolysis
n3:kodStatuVydavatele
US - Spojené státy americké
n3:kontrolniKodProRIV
[8DC8AD9F3B46]
n3:nazevZdroje
Industrial and Engineering Chemistry Research
n3:obor
n20:CI
n3:pocetDomacichTvurcuVysledku
3
n3:pocetTvurcuVysledku
5
n3:projekt
n15:GA104%2F09%2F0880
n3:rokUplatneniVysledku
n8:2012
n3:svazekPeriodika
51
n3:tvurceVysledku
Křišťál, Jiří Hanika, Jiří Jiřičný, Vladimír Bouzek, K. Kodým, R.
n3:wos
000300467100009
n3:zamer
n13:AV0Z40720504
s:issn
0888-5885
s:numberOfPages
10
n19:doi
10.1021/ie200654c