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Statements

Subject Item
n2:RIV%2F67985858%3A_____%2F03%3A27030253%21RIV%2F2004%2FGA0%2FA27004%2FN
rdf:type
skos:Concept n17:Vysledek
dcterms:description
The conformational behaviour of simple thiacalix[4]arene derivatives was studied using a combination of NMR spectroscopy and X-ray diffraction analysis. The 25,26,27,28-tetramethoxythiacalix[4]arene was found to adopt an unprecedented solid-state structure, where the cone and 1,3-alternate conformers co-exist in the crystal lattice in the 3:1 ratio. This phenomenon reflects the basically distinct conformational behaviour of thiacalix[4]arene skeleton as compared with classical calixarenes. The conformational behaviour of simple thiacalix[4]arene derivatives was studied using a combination of NMR spectroscopy and X-ray diffraction analysis. The 25,26,27,28-tetramethoxythiacalix[4]arene was found to adopt an unprecedented solid-state structure, where the cone and 1,3-alternate conformers co-exist in the crystal lattice in the 3:1 ratio. This phenomenon reflects the basically distinct conformational behaviour of thiacalix[4]arene skeleton as compared with classical calixarenes.
dcterms:title
Conformational Behaviour of Tetramethoxythiacalix[4]arenes: Solution versus Solid-State Study. Conformational Behaviour of Tetramethoxythiacalix[4]arenes: Solution versus Solid-State Study.
skos:prefLabel
Conformational Behaviour of Tetramethoxythiacalix[4]arenes: Solution versus Solid-State Study. Conformational Behaviour of Tetramethoxythiacalix[4]arenes: Solution versus Solid-State Study.
skos:notation
RIV/67985858:_____/03:27030253!RIV/2004/GA0/A27004/N
n3:strany
7581;7585
n3:aktivita
n5:P n5:Z
n3:aktivity
P(GA203/03/0926), Z(AV0Z4072921), Z(MSM 113200001)
n3:cisloPeriodika
38
n3:dodaniDat
n6:2004
n3:domaciTvurceVysledku
n18:6618669
n3:druhVysledku
n9:J
n3:duvernostUdaju
n16:S
n3:entitaPredkladatele
n7:predkladatel
n3:idSjednocenehoVysledku
602016
n3:idVysledku
RIV/67985858:_____/03:27030253
n3:jazykVysledku
n8:eng
n3:klicovaSlova
calixarenes; conformations; x-ray crystallography
n3:klicoveSlovo
n4:x-ray%20crystallography n4:calixarenes n4:conformations
n3:kodStatuVydavatele
GB - Spojené království Velké Británie a Severního Irska
n3:kontrolniKodProRIV
[06073323880C]
n3:nazevZdroje
Tetrahedron
n3:obor
n15:CF
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
7
n3:pocetUcastnikuAkce
0
n3:pocetZahranicnichUcastnikuAkce
0
n3:projekt
n14:GA203%2F03%2F0926
n3:rokUplatneniVysledku
n6:2003
n3:svazekPeriodika
59
n3:tvurceVysledku
Dvořáková, H. Petříčková, H. Lhoták, P. Lang, J. Stibor, I. Himl, M. Sýkora, Jan
n3:zamer
n12:AV0Z4072921 n12:MSM%20113200001
s:issn
0040-4020
s:numberOfPages
5