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Statements

Subject Item
n2:RIV%2F62690094%3A18470%2F12%3A50000943%21RIV13-MSM-18470___
rdf:type
n10:Vysledek skos:Concept
dcterms:description
4,6-Diazido-N-nitro-1,3,5-triazine-2-amine (DANT) was prepared with a 35% yield from cyanuric chloride in a three step process. DANT was characterized by IR and NMR spectroscopy (1H, 13C, 15N), single-crystal X-ray diffraction, and DTA. The crystal density of DANT is 1.849 gcm_3. The cyclization of one azido group and one nitrogen atom of the triazine group giving tetrazole was observed for DANT in a dimethyl sulfoxide solution using NMR spectroscopy. An equilibrium exists between the original DANT molecule and its cyclic form at a ratio of 7 : 3. The sensitivity of DANT to impact is between that for PETN and RDX, sensitivity to friction is between that for lead azide and PETN, and sensitivity to electric discharge is about the same as for PETN. DANT’s heat of combustion is 2060 kJmol_1. 4,6-Diazido-N-nitro-1,3,5-triazine-2-amine (DANT) was prepared with a 35% yield from cyanuric chloride in a three step process. DANT was characterized by IR and NMR spectroscopy (1H, 13C, 15N), single-crystal X-ray diffraction, and DTA. The crystal density of DANT is 1.849 gcm_3. The cyclization of one azido group and one nitrogen atom of the triazine group giving tetrazole was observed for DANT in a dimethyl sulfoxide solution using NMR spectroscopy. An equilibrium exists between the original DANT molecule and its cyclic form at a ratio of 7 : 3. The sensitivity of DANT to impact is between that for PETN and RDX, sensitivity to friction is between that for lead azide and PETN, and sensitivity to electric discharge is about the same as for PETN. DANT’s heat of combustion is 2060 kJmol_1.
dcterms:title
Characterization of 4,6-diazido-N-nitro-1,3,5-triazine-2-amine Characterization of 4,6-diazido-N-nitro-1,3,5-triazine-2-amine
skos:prefLabel
Characterization of 4,6-diazido-N-nitro-1,3,5-triazine-2-amine Characterization of 4,6-diazido-N-nitro-1,3,5-triazine-2-amine
skos:notation
RIV/62690094:18470/12:50000943!RIV13-MSM-18470___
n10:predkladatel
n11:orjk%3A18470
n3:aktivita
n13:Z n13:I
n3:aktivity
I, Z(MSM0021627501)
n3:cisloPeriodika
3
n3:dodaniDat
n16:2013
n3:domaciTvurceVysledku
n12:7296126
n3:druhVysledku
n15:J
n3:duvernostUdaju
n9:S
n3:entitaPredkladatele
n14:predkladatel
n3:idSjednocenehoVysledku
126854
n3:idVysledku
RIV/62690094:18470/12:50000943
n3:jazykVysledku
n18:eng
n3:klicovaSlova
X-ray diffraction; NMR spectroscopy; DANT; 4,6-Diazido-N-nitro-1,3,5-triazine-2-amine
n3:klicoveSlovo
n4:NMR%20spectroscopy n4:4 n4:X-ray%20diffraction n4:5-triazine-2-amine n4:3 n4:6-Diazido-N-nitro-1 n4:DANT
n3:kodStatuVydavatele
DE - Spolková republika Německo
n3:kontrolniKodProRIV
[FD0B5C1D1283]
n3:nazevZdroje
Propellants, explosives, pyrotechnics
n3:obor
n20:CC
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
4
n3:rokUplatneniVysledku
n16:2012
n3:svazekPeriodika
37
n3:tvurceVysledku
Matyáš, Robert Lyčka, Antonín Musil, Tomáš Růžička, Aleš
n3:wos
000305247000005
n3:zamer
n7:MSM0021627501
s:issn
0721-3115
s:numberOfPages
7
n19:doi
10.1002/prep.201000166
n5:organizacniJednotka
18470