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Statements

Subject Item
n2:RIV%2F62156489%3A43210%2F04%3A00000324%21RIV%2F2005%2FGA0%2F432105%2FN
rdf:type
skos:Concept n13:Vysledek
dcterms:description
Abstrakt A newly elaborated accelerated solvent extraction (ASE) procedure allowed more accurate (<2%) and precise (<5-8% rel.) HPLC/UV/MS determination of isoflavones in different kinds of food made from soybean (products of ecological agriculture), i.e. soy farina, soy meat granulate, soy meat laminae, soy meat bits, Protmix and EKO-B1. The on-column limits of detection (LOD) for daidzin/genistin were 1.2/1.6 fmol for the signal-to-noise ratio S/N = 3 and 1-3 fmol for daidzem, genistein, formononetin, biochanin A and ononin, respectively. Final concentrations of daidzin in soybean foods fluctuated between 30 and 60 mug/g of dry matter (DM). Significantly higher concentrations of genistin (between 60 and 130 mug/g DM) were found in the soybean foods. A newly elaborated accelerated solvent extraction (ASE) procedure allowed more accurate (<2%) and precise (<5-8% rel.) HPLC/UV/MS determination of isoflavones in different kinds of food made from soybean (products of ecological agriculture), i.e. soy farina, soy meat granulate, soy meat laminae, soy meat bits, Protmix and EKO-B1. The on-column limits of detection (LOD) for daidzin/genistin were 1.2/1.6 fmol for the signal-to-noise ratio S/N = 3 and 1-3 fmol for daidzem, genistein, formononetin, biochanin A and ononin, respectively. Final concentrations of daidzin in soybean foods fluctuated between 30 and 60 mug/g of dry matter (DM). Significantly higher concentrations of genistin (between 60 and 130 mug/g DM) were found in the soybean foods.
dcterms:title
Liquid chromatographic-mass spectrometric determination of genistin and daidzin in soybean food samples after accelerated solvent extraction with modified content of extraction cell HPLC/MS stanovení genistinu a daidzinu v potravinách na bázi sojových bobů Liquid chromatographic-mass spectrometric determination of genistin and daidzin in soybean food samples after accelerated solvent extraction with modified content of extraction cell
skos:prefLabel
Liquid chromatographic-mass spectrometric determination of genistin and daidzin in soybean food samples after accelerated solvent extraction with modified content of extraction cell Liquid chromatographic-mass spectrometric determination of genistin and daidzin in soybean food samples after accelerated solvent extraction with modified content of extraction cell HPLC/MS stanovení genistinu a daidzinu v potravinách na bázi sojových bobů
skos:notation
RIV/62156489:43210/04:00000324!RIV/2005/GA0/432105/N
n3:strany
1;11
n3:aktivita
n4:P
n3:aktivity
P(GA521/02/1367)
n3:cisloPeriodika
1-2
n3:dodaniDat
n6:2005
n3:domaciTvurceVysledku
n5:1150936 n5:8683913 n5:4186559 n5:2645572 n5:3363104 n5:4995775
n3:druhVysledku
n18:J
n3:duvernostUdaju
n11:S
n3:entitaPredkladatele
n17:predkladatel
n3:idSjednocenehoVysledku
571625
n3:idVysledku
RIV/62156489:43210/04:00000324
n3:jazykVysledku
n15:eng
n3:klicovaSlova
Soxhlet extraction;UV spectrophotometric detection;accelerated solvent extraction;daidzin;foodstuffs;genistin;high-performance liquid chromatography;isoflavones;mass spectrometry;solvent extraction;soybean food;ultrasonic extraction
n3:klicoveSlovo
n9:daidzin n9:foodstuffs n9:genistin n9:accelerated%20solvent%20extraction n9:UV%20spectrophotometric%20detection n9:soybean%20food n9:high-performance%20liquid%20chromatography n9:isoflavones n9:solvent%20extraction n9:ultrasonic%20extraction n9:mass%20spectrometry n9:Soxhlet%20extraction
n3:kodStatuVydavatele
NL - Nizozemsko
n3:kontrolniKodProRIV
[A68558BE9338]
n3:nazevZdroje
Analytica Chimica Acta
n3:obor
n14:CB
n3:pocetDomacichTvurcuVysledku
6
n3:pocetTvurcuVysledku
7
n3:projekt
n12:GA521%2F02%2F1367
n3:rokUplatneniVysledku
n6:2004
n3:svazekPeriodika
517
n3:tvurceVysledku
Mikelová, Radka Klejdus, Bořivoj Adam, Vojtěch Zehnálek, Josef Kízek, René Vacek, Jan Kubáň, Vlastimil
s:issn
0003-2670
s:numberOfPages
11
n16:organizacniJednotka
43210