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Statements

Subject Item
n2:RIV%2F61989592%3A15310%2F14%3A33151963%21RIV15-MSM-15310___
rdf:type
skos:Concept n13:Vysledek
rdfs:seeAlso
http://pubs.acs.org/doi/pdf/10.1021/co500084k
dcterms:description
The solid-phase synthesis of trisubstituted 2,5-dihydrobenzo[f]thiadiazepine 1,1-dioxides is reported. Acyclic polymer-supported intermediates were prepared using commercially available building blocks: Fmoc-protected amino acids, 2-nitrobenzenesulfonyl chlorides, and bromoketones. The acyclic precursors underwent acid-mediated release from the resin and the cyclization was completed in solution. The solid-phase synthesis of trisubstituted 2,5-dihydrobenzo[f]thiadiazepine 1,1-dioxides is reported. Acyclic polymer-supported intermediates were prepared using commercially available building blocks: Fmoc-protected amino acids, 2-nitrobenzenesulfonyl chlorides, and bromoketones. The acyclic precursors underwent acid-mediated release from the resin and the cyclization was completed in solution.
dcterms:title
Solid-Phase Synthesis of Trisubstituted 2,5-Dihydrobenzo[f]thiadiazepine 1,1-Dioxide Derivatives Solid-Phase Synthesis of Trisubstituted 2,5-Dihydrobenzo[f]thiadiazepine 1,1-Dioxide Derivatives
skos:prefLabel
Solid-Phase Synthesis of Trisubstituted 2,5-Dihydrobenzo[f]thiadiazepine 1,1-Dioxide Derivatives Solid-Phase Synthesis of Trisubstituted 2,5-Dihydrobenzo[f]thiadiazepine 1,1-Dioxide Derivatives
skos:notation
RIV/61989592:15310/14:33151963!RIV15-MSM-15310___
n3:aktivita
n9:P
n3:aktivity
P(EE2.4.31.0130), P(GAP207/12/0473)
n3:cisloPeriodika
8
n3:dodaniDat
n19:2015
n3:domaciTvurceVysledku
n12:4422759 n12:5355346
n3:druhVysledku
n6:J
n3:duvernostUdaju
n15:S
n3:entitaPredkladatele
n14:predkladatel
n3:idSjednocenehoVysledku
45895
n3:idVysledku
RIV/61989592:15310/14:33151963
n3:jazykVysledku
n18:eng
n3:klicovaSlova
amino acids, benzothiadiazepines, bromoketones, cyclative cleavage, nitrobenzenesulfonyl chlorides, solid-phase synthesis
n3:klicoveSlovo
n5:amino%20acids n5:bromoketones n5:cyclative%20cleavage n5:benzothiadiazepines n5:solid-phase%20synthesis n5:nitrobenzenesulfonyl%20chlorides
n3:kodStatuVydavatele
US - Spojené státy americké
n3:kontrolniKodProRIV
[466B438E232B]
n3:nazevZdroje
ACS Combinatorial Science
n3:obor
n16:CC
n3:pocetDomacichTvurcuVysledku
2
n3:pocetTvurcuVysledku
2
n3:projekt
n4:GAP207%2F12%2F0473 n4:EE2.4.31.0130
n3:rokUplatneniVysledku
n19:2014
n3:svazekPeriodika
16
n3:tvurceVysledku
Fülöpová, Veronika Krchňák, Viktor
n3:wos
000340344500007
s:issn
2156-8952
s:numberOfPages
9
n17:doi
10.1021/co500084k
n10:organizacniJednotka
15310