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Statements

Subject Item
n2:RIV%2F61989592%3A15310%2F14%3A33151903%21RIV15-MSM-15310___
rdf:type
skos:Concept n13:Vysledek
rdfs:seeAlso
http://pubs.acs.org/doi/pdf/10.1021/co5000163
dcterms:description
The stereoselective synthesis of 1,2,11,11a-tetrahydrobenzo[e]pyrazinothiadiazin-3(4H)-one 6,6-dioxides on a solid support via tandem N-sulfonyl iminium ion cyclization, followed by nucleophilic addition is reported. The synthesis proceeded with full control of stereoselectivity at the newly formed asymmetric carbon, under mild conditions, and using commercially available building blocks. The synthetic route provided high-purity crude products. The stereoselective synthesis of 1,2,11,11a-tetrahydrobenzo[e]pyrazinothiadiazin-3(4H)-one 6,6-dioxides on a solid support via tandem N-sulfonyl iminium ion cyclization, followed by nucleophilic addition is reported. The synthesis proceeded with full control of stereoselectivity at the newly formed asymmetric carbon, under mild conditions, and using commercially available building blocks. The synthetic route provided high-purity crude products.
dcterms:title
Polymer-?Supported Stereoselective Synthesis of Tetrahydrobenzopyrazino-?thiadiazinone Dioxides via N-?Sulfonyl Iminiums Polymer-?Supported Stereoselective Synthesis of Tetrahydrobenzopyrazino-?thiadiazinone Dioxides via N-?Sulfonyl Iminiums
skos:prefLabel
Polymer-?Supported Stereoselective Synthesis of Tetrahydrobenzopyrazino-?thiadiazinone Dioxides via N-?Sulfonyl Iminiums Polymer-?Supported Stereoselective Synthesis of Tetrahydrobenzopyrazino-?thiadiazinone Dioxides via N-?Sulfonyl Iminiums
skos:notation
RIV/61989592:15310/14:33151903!RIV15-MSM-15310___
n4:aktivita
n17:P
n4:aktivity
P(ED0030/01/01), P(EE2.3.20.0009), P(GAP207/12/0473)
n4:cisloPeriodika
6
n4:dodaniDat
n9:2015
n4:domaciTvurceVysledku
n11:4422759 n11:3143120 La Venia, Agustina
n4:druhVysledku
n18:J
n4:duvernostUdaju
n20:S
n4:entitaPredkladatele
n10:predkladatel
n4:idSjednocenehoVysledku
37430
n4:idVysledku
RIV/61989592:15310/14:33151903
n4:jazykVysledku
n8:eng
n4:klicovaSlova
sp3 carbon; tetrahydrobenzopyrazinothiadiazinone; stereoselective; polymer-supported; N-sulfonyl iminiums
n4:klicoveSlovo
n12:sp3%20carbon n12:N-sulfonyl%20iminiums n12:polymer-supported n12:tetrahydrobenzopyrazinothiadiazinone n12:stereoselective
n4:kodStatuVydavatele
US - Spojené státy americké
n4:kontrolniKodProRIV
[5C457E6FC22B]
n4:nazevZdroje
ACS Combinatorial Science
n4:obor
n19:CC
n4:pocetDomacichTvurcuVysledku
3
n4:pocetTvurcuVysledku
3
n4:projekt
n6:ED0030%2F01%2F01 n6:GAP207%2F12%2F0473 n6:EE2.3.20.0009
n4:rokUplatneniVysledku
n9:2014
n4:svazekPeriodika
16
n4:tvurceVysledku
Cankařová, Naděžda La Venia, Agustina Krchňák, Viktor
n4:wos
000337121600005
s:issn
2156-8952
s:numberOfPages
10
n16:doi
10.1021/co5000163
n7:organizacniJednotka
15310