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Statements

Subject Item
n2:RIV%2F61989592%3A15310%2F10%3A10215253%21RIV11-MSM-15310___
rdf:type
n9:Vysledek skos:Concept
dcterms:description
This paper deals with a simple and low-cost method developed to deposit hematite (alfa-Fe2O3) layers on a fluorine-doped tin oxide (FTO/F:SnO2) substrate by thermal decomposition of solid iron(III) chloride hexahydrate (FeCl3?6H2O). Deposition procedure takes place through chemical intermediate iron(III) oxide chloride (FeOCl) film. A crucial influence of atmosphere dynamics involved in the calcination process of FeOCl has been observed. As-deposited films were characterized by means of Conversion Electron Mössbauer Spectroscopy (CEMS), Grazing Angle X-Ray Diffractometry (GAXRD), Atomic Force Microscopy (AFM), Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray (EDX) analysis. Final nanocrystalline hematite film with a cactus-field-like design consists of 20 nm thick porous crystal plates. A process of hematite doping by tin atoms from substrate coating is also discussed. This paper deals with a simple and low-cost method developed to deposit hematite (alfa-Fe2O3) layers on a fluorine-doped tin oxide (FTO/F:SnO2) substrate by thermal decomposition of solid iron(III) chloride hexahydrate (FeCl3?6H2O). Deposition procedure takes place through chemical intermediate iron(III) oxide chloride (FeOCl) film. A crucial influence of atmosphere dynamics involved in the calcination process of FeOCl has been observed. As-deposited films were characterized by means of Conversion Electron Mössbauer Spectroscopy (CEMS), Grazing Angle X-Ray Diffractometry (GAXRD), Atomic Force Microscopy (AFM), Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray (EDX) analysis. Final nanocrystalline hematite film with a cactus-field-like design consists of 20 nm thick porous crystal plates. A process of hematite doping by tin atoms from substrate coating is also discussed.
dcterms:title
A nanocrystalline hematite film prepared from iron(III) chloride precursor A nanocrystalline hematite film prepared from iron(III) chloride precursor
skos:prefLabel
A nanocrystalline hematite film prepared from iron(III) chloride precursor A nanocrystalline hematite film prepared from iron(III) chloride precursor
skos:notation
RIV/61989592:15310/10:10215253!RIV11-MSM-15310___
n4:aktivita
n16:Z n16:P
n4:aktivity
P(1M0512), P(KAN101630651), Z(MSM6198959218)
n4:cisloPeriodika
518
n4:dodaniDat
n5:2011
n4:domaciTvurceVysledku
n6:1356194 n6:7321023 n6:8570647 n6:7266065 n6:3883620 n6:9317708 n6:1490397
n4:druhVysledku
n17:J
n4:duvernostUdaju
n12:S
n4:entitaPredkladatele
n15:predkladatel
n4:idSjednocenehoVysledku
244718
n4:idVysledku
RIV/61989592:15310/10:10215253
n4:jazykVysledku
n18:eng
n4:klicovaSlova
Nanostructures; Mössbauer spectroscopy; Iron oxide; Hydrogen; Heat treatment; Deposition process
n4:klicoveSlovo
n11:Nanostructures n11:M%C3%B6ssbauer%20spectroscopy n11:Hydrogen n11:Deposition%20process n11:Iron%20oxide n11:Heat%20treatment
n4:kodStatuVydavatele
CH - Švýcarská konfederace
n4:kontrolniKodProRIV
[DD3228121AFD]
n4:nazevZdroje
Thin Solid Films
n4:obor
n19:BM
n4:pocetDomacichTvurcuVysledku
7
n4:pocetTvurcuVysledku
8
n4:projekt
n14:1M0512 n14:KAN101630651
n4:rokUplatneniVysledku
n5:2010
n4:svazekPeriodika
21
n4:tvurceVysledku
Sharma, Virender K. Machala, Libor Heřmánek, Martin Mašláň, Miroslav Pechoušek, Jiří Medřík, Ivo Frydrych, Jiří Tuček, Jiří
n4:wos
000280989100008
n4:zamer
n7:MSM6198959218
s:issn
0040-6090
s:numberOfPages
4
n13:organizacniJednotka
15310