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Statements

Subject Item
n2:RIV%2F61989592%3A15310%2F08%3A00005798%21RIV10-MSM-15310___
rdf:type
n15:Vysledek skos:Concept
dcterms:description
A library of negative ion electrospray ionization mass spectra and tandem mass spectra (MS/MS) of sulfonated dyes has been developed for fast identification purposes. The uniform protocol has been elaborated and applied to the measurements of more than 50 anionic dyes. Three collision energies are selected in our protocol which ensures that at least one of them provides a suitable ratio of product ions to the precursor ion. The robustness is investigated with altered values of tuning parameters (e.g. the pressure of the nebulizing gas, the temperature and the flow rate of drying gas, and the mobile phase composition). The results of the inter-laboratory comparison of product ion mass spectra recorded on seven different tandem mass spectrometers (three ion traps, two triple quadrupoles and two hybrid quadrupole time of flight instruments) are presented for four representative anionic dyes - azo dye Acid Red 118, anthraquinone dye Acid Violet 43, triphenylmethane dye Acid Blue 1 and AMID metal-complex a A library of negative ion electrospray ionization mass spectra and tandem mass spectra (MS/MS) of sulfonated dyes has been developed for fast identification purposes. The uniform protocol has been elaborated and applied to the measurements of more than 50 anionic dyes. Three collision energies are selected in our protocol which ensures that at least one of them provides a suitable ratio of product ions to the precursor ion. The robustness is investigated with altered values of tuning parameters (e.g. the pressure of the nebulizing gas, the temperature and the flow rate of drying gas, and the mobile phase composition). The results of the inter-laboratory comparison of product ion mass spectra recorded on seven different tandem mass spectrometers (three ion traps, two triple quadrupoles and two hybrid quadrupole time of flight instruments) are presented for four representative anionic dyes - azo dye Acid Red 118, anthraquinone dye Acid Violet 43, triphenylmethane dye Acid Blue 1 and AMID metal-complex a
dcterms:title
Comparison of negative ion electrospray mass spectra measured by seven tandem mass analyzers towards library formation Comparison of negative ion electrospray mass spectra measured by seven tandem mass analyzers towards library formation
skos:prefLabel
Comparison of negative ion electrospray mass spectra measured by seven tandem mass analyzers towards library formation Comparison of negative ion electrospray mass spectra measured by seven tandem mass analyzers towards library formation
skos:notation
RIV/61989592:15310/08:00005798!RIV10-MSM-15310___
n3:aktivita
n6:P n6:Z
n3:aktivity
P(IAA4031104), P(OPUOFVZ200602), Z(MSM6046137301), Z(MSM6046137305), Z(MSM6198959216)
n3:cisloPeriodika
2
n3:dodaniDat
n14:2010
n3:domaciTvurceVysledku
n17:4316851
n3:druhVysledku
n8:J
n3:duvernostUdaju
n11:S
n3:entitaPredkladatele
n10:predkladatel
n3:idSjednocenehoVysledku
360623
n3:idVysledku
RIV/61989592:15310/08:00005798
n3:jazykVysledku
n18:eng
n3:klicovaSlova
chromatography/mass spectrometry instruments; collisionally induced dissociation; liquid-chromatography; sulfonated dyes; azo dyestuffs; ionization; drugs; TRAP; identification; searching
n3:klicoveSlovo
n4:identification n4:collisionally%20induced%20dissociation n4:chromatography%2Fmass%20spectrometry%20instruments n4:sulfonated%20dyes n4:drugs n4:liquid-chromatography n4:searching n4:azo%20dyestuffs n4:ionization n4:TRAP
n3:kodStatuVydavatele
GB - Spojené království Velké Británie a Severního Irska
n3:kontrolniKodProRIV
[D6593496D004]
n3:nazevZdroje
Rapid Communications in Mass Spectrometry
n3:obor
n19:CB
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
8
n3:projekt
n13:IAA4031104 n13:OPUOFVZ200602
n3:rokUplatneniVysledku
n14:2008
n3:svazekPeriodika
22
n3:tvurceVysledku
Volná, Kateřina Poustka, Jan Čáslavský, Josef Kačer, Petr Holčapek, Michal Kolářová, Lenka Lemr, Karel Hubálek, Martin
n3:zamer
n9:MSM6198959216 n9:MSM6046137301 n9:MSM6046137305
s:issn
0951-4198
s:numberOfPages
8
n7:organizacniJednotka
15310