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Statements

Subject Item
n2:RIV%2F61388980%3A_____%2F12%3A00379816%21RIV13-AV0-61388980
rdf:type
n6:Vysledek skos:Concept
dcterms:description
Manganese(IV) oxides were prepared by homogeneous hydrolysis of potassium permanganate with 2-chloroacetamide and direct reaction of potassium permanganate with manganese(II) sulfate in aqueous solutions. Synthesized manganese(IV) oxides were characterized using Brunauer-Emmett-Teller (BET) surface area and Barrett-Joiner-Halenda porosity (BJH), X-ray diffraction (XRD), infrared spectroscopy (IR), and scanning electron microscopy (SEM). These oxides were taken for an experimental evaluation of their reactivity with sulfur mustard (HD or bis(2-Chloroethyl)sulfide), soman (GD or (3,3'-dimethylbutan-2-yl)-) and VX agent (S-[-(diisopropylamino)ethyl]-O-ethyl-methylphosphonothionate). The degree of conversion for sulfur mustard and agent VX is very good for both samples and come up to 95% and 99%, respectively. In the contrast to sulfur mustard and agent VX, degradation of soman was only 56% of the cryptomelane-type MnO2 and 18% of the birnessite-type MnO2. Manganese(IV) oxides were prepared by homogeneous hydrolysis of potassium permanganate with 2-chloroacetamide and direct reaction of potassium permanganate with manganese(II) sulfate in aqueous solutions. Synthesized manganese(IV) oxides were characterized using Brunauer-Emmett-Teller (BET) surface area and Barrett-Joiner-Halenda porosity (BJH), X-ray diffraction (XRD), infrared spectroscopy (IR), and scanning electron microscopy (SEM). These oxides were taken for an experimental evaluation of their reactivity with sulfur mustard (HD or bis(2-Chloroethyl)sulfide), soman (GD or (3,3'-dimethylbutan-2-yl)-) and VX agent (S-[-(diisopropylamino)ethyl]-O-ethyl-methylphosphonothionate). The degree of conversion for sulfur mustard and agent VX is very good for both samples and come up to 95% and 99%, respectively. In the contrast to sulfur mustard and agent VX, degradation of soman was only 56% of the cryptomelane-type MnO2 and 18% of the birnessite-type MnO2.
dcterms:title
Mesoporous manganese oxide for warfare agents degradation Mesoporous manganese oxide for warfare agents degradation
skos:prefLabel
Mesoporous manganese oxide for warfare agents degradation Mesoporous manganese oxide for warfare agents degradation
skos:notation
RIV/61388980:_____/12:00379816!RIV13-AV0-61388980
n6:predkladatel
n17:ico%3A61388980
n3:aktivita
n14:P n14:Z
n3:aktivity
P(FI-IM5/231), Z(AV0Z40320502), Z(AV0Z40500505)
n3:cisloPeriodika
JULY
n3:dodaniDat
n10:2013
n3:domaciTvurceVysledku
n7:7549393
n3:druhVysledku
n15:J
n3:duvernostUdaju
n18:S
n3:entitaPredkladatele
n20:predkladatel
n3:idSjednocenehoVysledku
149565
n3:idVysledku
RIV/61388980:_____/12:00379816
n3:jazykVysledku
n9:eng
n3:klicovaSlova
homogeneous hydrolysis; chloroacetamide; manganese(IV) oxide; warfare agents
n3:klicoveSlovo
n4:homogeneous%20hydrolysis n4:manganese%28IV%29%20oxide n4:warfare%20agents n4:chloroacetamide
n3:kodStatuVydavatele
NL - Nizozemsko
n3:kontrolniKodProRIV
[79E0FE973FBA]
n3:nazevZdroje
Microporous and Mesoporous Materials
n3:obor
n5:CA
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
4
n3:projekt
n13:FI-IM5%2F231
n3:rokUplatneniVysledku
n10:2012
n3:svazekPeriodika
156
n3:tvurceVysledku
Němec, T. Králová, Daniela Opluštil, F. Štengl, Václav
n3:wos
000303625200032
n3:zamer
n11:AV0Z40320502 n11:AV0Z40500505
s:issn
1387-1811
s:numberOfPages
9
n8:doi
10.1016/j.micromeso.2012.02.031