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Statements

Subject Item
n2:RIV%2F61388980%3A_____%2F11%3A00370934%21RIV12-AV0-61388980
rdf:type
n11:Vysledek skos:Concept
dcterms:description
Titanium(IV)-manganese(IV) nano-dispersed oxides were prepared by a homogeneous hydrolysis of potassium permanganate and titanium(IV) oxo-sulphate with 2-chloroacetamide. Synthesised samples were characterised using Brunauer-Emmett-Teller (BET) surface area and Barrett-Joiner-Halenda porosity (BJH), X-ray diffraction (XRD), infrared spectroscopy (IR), and scanning electron microscopy (SEM). These oxides were taken for an experimental evaluation of their reactivity with sulphur mustard (HD or bis(2-chloroethyl)sulphide) and soman (GD or (3,3'-dimethylbutan-2-yl)-methylphosphono-fluoridate). Mn(4+) content affects the decontamination activity; with increasing Mn(4+) content the activity increases for sulphur mustard and decreases for soman. The best decontamination activities for sulphur mustard and soman were observed for samples TiMn_37 with 18.6 wt.% Mn and TiMn_5 with 2.1 wt.% Mn, respectively. Titanium(IV)-manganese(IV) nano-dispersed oxides were prepared by a homogeneous hydrolysis of potassium permanganate and titanium(IV) oxo-sulphate with 2-chloroacetamide. Synthesised samples were characterised using Brunauer-Emmett-Teller (BET) surface area and Barrett-Joiner-Halenda porosity (BJH), X-ray diffraction (XRD), infrared spectroscopy (IR), and scanning electron microscopy (SEM). These oxides were taken for an experimental evaluation of their reactivity with sulphur mustard (HD or bis(2-chloroethyl)sulphide) and soman (GD or (3,3'-dimethylbutan-2-yl)-methylphosphono-fluoridate). Mn(4+) content affects the decontamination activity; with increasing Mn(4+) content the activity increases for sulphur mustard and decreases for soman. The best decontamination activities for sulphur mustard and soman were observed for samples TiMn_37 with 18.6 wt.% Mn and TiMn_5 with 2.1 wt.% Mn, respectively.
dcterms:title
Mesoporous titanium-manganese dioxide for sulphur mustard and soman decontamination Mesoporous titanium-manganese dioxide for sulphur mustard and soman decontamination
skos:prefLabel
Mesoporous titanium-manganese dioxide for sulphur mustard and soman decontamination Mesoporous titanium-manganese dioxide for sulphur mustard and soman decontamination
skos:notation
RIV/61388980:_____/11:00370934!RIV12-AV0-61388980
n11:predkladatel
n12:ico%3A61388980
n3:aktivita
n15:Z n15:P
n3:aktivity
P(GA203/08/0334), Z(AV0Z40320502)
n3:cisloPeriodika
11
n3:dodaniDat
n20:2012
n3:domaciTvurceVysledku
n10:5875994 n10:7549393
n3:druhVysledku
n18:J
n3:duvernostUdaju
n8:S
n3:entitaPredkladatele
n17:predkladatel
n3:idSjednocenehoVysledku
211650
n3:idVysledku
RIV/61388980:_____/11:00370934
n3:jazykVysledku
n19:eng
n3:klicovaSlova
oxides; chemical synthesis; X-Ray diffraction; raman spectroscopy; infrared spectroscopy
n3:klicoveSlovo
n4:raman%20spectroscopy n4:chemical%20synthesis n4:infrared%20spectroscopy n4:X-Ray%20diffraction n4:oxides
n3:kodStatuVydavatele
GB - Spojené království Velké Británie a Severního Irska
n3:kontrolniKodProRIV
[3B5D88059DCB]
n3:nazevZdroje
Materials Research Bulletin
n3:obor
n7:CA
n3:pocetDomacichTvurcuVysledku
2
n3:pocetTvurcuVysledku
4
n3:projekt
n16:GA203%2F08%2F0334
n3:rokUplatneniVysledku
n20:2011
n3:svazekPeriodika
46
n3:tvurceVysledku
Bludská, Jana Opluštil, F. Němec, T. Štengl, Václav
n3:wos
000296038700053
n3:zamer
n14:AV0Z40320502
s:issn
0025-5408
s:numberOfPages
7
n6:doi
10.1016/j.materresbull.2011.07.003