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Statements

Subject Item
n2:RIV%2F61388980%3A_____%2F11%3A00370205%21RIV12-AV0-61388980
rdf:type
skos:Concept n14:Vysledek
dcterms:description
The effectiveness of Raman spectroscopy (using a bench-top system on standard pigments) for the characterisation of modified lead antimonate yellows was demonstrated in the already published Part I. The knowledge gained is employed here for the study of yellow glazes on genuine Renaissance plates with the aim of identifying non-invasively lead pyroantimonate compounds by portable micro-Raman equipment. The investigation was carried out directly on site, at the Victoria and Albert Museum (London, UK) and at the Museo Statale d'Arte Medievale di Arezzo (Arezzo, Italy), combining Raman and X-ray fluorescence analyses. In addition to the spectral features of both unmodified Naples yellow and Sn- and Zn-modified lead antimonate compounds, the Raman patterns related to partially modified pyrochlore structures were observed. For this reason, the possible Sn-induced modification of Naples yellow by cassiterite (SnO(2)), present within the glaze as opacifier was explored on lead antimonate yellow glaze mock-ups fired at different temperatures. The effectiveness of Raman spectroscopy (using a bench-top system on standard pigments) for the characterisation of modified lead antimonate yellows was demonstrated in the already published Part I. The knowledge gained is employed here for the study of yellow glazes on genuine Renaissance plates with the aim of identifying non-invasively lead pyroantimonate compounds by portable micro-Raman equipment. The investigation was carried out directly on site, at the Victoria and Albert Museum (London, UK) and at the Museo Statale d'Arte Medievale di Arezzo (Arezzo, Italy), combining Raman and X-ray fluorescence analyses. In addition to the spectral features of both unmodified Naples yellow and Sn- and Zn-modified lead antimonate compounds, the Raman patterns related to partially modified pyrochlore structures were observed. For this reason, the possible Sn-induced modification of Naples yellow by cassiterite (SnO(2)), present within the glaze as opacifier was explored on lead antimonate yellow glaze mock-ups fired at different temperatures.
dcterms:title
Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In situ characterisation of Renaissance plates by portable micro-Raman and XRF studies Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In situ characterisation of Renaissance plates by portable micro-Raman and XRF studies
skos:prefLabel
Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In situ characterisation of Renaissance plates by portable micro-Raman and XRF studies Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In situ characterisation of Renaissance plates by portable micro-Raman and XRF studies
skos:notation
RIV/61388980:_____/11:00370205!RIV12-AV0-61388980
n14:predkladatel
n15:ico%3A61388980
n4:aktivita
n5:Z
n4:aktivity
Z(AV0Z40320502)
n4:cisloPeriodika
3
n4:dodaniDat
n6:2012
n4:domaciTvurceVysledku
n7:4208994 n7:7933665
n4:druhVysledku
n11:J
n4:duvernostUdaju
n19:S
n4:entitaPredkladatele
n18:predkladatel
n4:idSjednocenehoVysledku
225648
n4:idVysledku
RIV/61388980:_____/11:00370205
n4:jazykVysledku
n12:eng
n4:klicovaSlova
Naples yellow; lead antimonate; cubic pyrochlore; non-invasive; in situ
n4:klicoveSlovo
n8:cubic%20pyrochlore n8:lead%20antimonate n8:non-invasive n8:in%20situ n8:Naples%20yellow
n4:kodStatuVydavatele
GB - Spojené království Velké Británie a Severního Irska
n4:kontrolniKodProRIV
[025289652544]
n4:nazevZdroje
Journal of Raman Spectroscopy
n4:obor
n13:DD
n4:pocetDomacichTvurcuVysledku
2
n4:pocetTvurcuVysledku
9
n4:rokUplatneniVysledku
n6:2011
n4:svazekPeriodika
42
n4:tvurceVysledku
Brunetti, B. G. Rosi, F. Miliani, C. Burgio, L. Sgamellotti, A. Bezdička, Petr Grygar, Tomáš Seccaroni, C. Manuali, V.
n4:wos
000288544000023
n4:zamer
n16:AV0Z40320502
s:issn
0377-0486
s:numberOfPages
8
n17:doi
10.1002/jrs.2699