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Statements

Subject Item
n2:RIV%2F61388963%3A_____%2F10%3A00347360%21RIV11-AV0-61388963
rdf:type
skos:Concept n17:Vysledek
dcterms:description
NMR study (NOESY, TOCSY, H-1-C-13 HSQC spectra) of analogues of oxytocin and deaminoocytocin having in position 7 L- or D-Tic is presented. The existence of both cis and trans configurations of the Cys(6)-D-Tic(7) bond is supported by observation of two sets of cross-peaks for H-1 and C-13 nuclei for most of the residues of the peptide not only in NOESY and TOCSY but also in H-1-C-13 HSQC spectra. The MS and HPLC indicate the presence of a single molecule/peptide, and NMR data thus suggest that this second set of peaks is due to the cis conformation. NMR study (NOESY, TOCSY, H-1-C-13 HSQC spectra) of analogues of oxytocin and deaminoocytocin having in position 7 L- or D-Tic is presented. The existence of both cis and trans configurations of the Cys(6)-D-Tic(7) bond is supported by observation of two sets of cross-peaks for H-1 and C-13 nuclei for most of the residues of the peptide not only in NOESY and TOCSY but also in H-1-C-13 HSQC spectra. The MS and HPLC indicate the presence of a single molecule/peptide, and NMR data thus suggest that this second set of peaks is due to the cis conformation.
dcterms:title
In position 7 l- and d-Tic-substituted oxytocin and deamino oxytocin: NMR study and conformational insights In position 7 l- and d-Tic-substituted oxytocin and deamino oxytocin: NMR study and conformational insights
skos:prefLabel
In position 7 l- and d-Tic-substituted oxytocin and deamino oxytocin: NMR study and conformational insights In position 7 l- and d-Tic-substituted oxytocin and deamino oxytocin: NMR study and conformational insights
skos:notation
RIV/61388963:_____/10:00347360!RIV11-AV0-61388963
n3:aktivita
n4:Z
n3:aktivity
Z(AV0Z40550506)
n3:cisloPeriodika
2
n3:dodaniDat
n7:2011
n3:domaciTvurceVysledku
n13:5602955 n13:3677672
n3:druhVysledku
n10:J
n3:duvernostUdaju
n9:S
n3:entitaPredkladatele
n12:predkladatel
n3:idSjednocenehoVysledku
263273
n3:idVysledku
RIV/61388963:_____/10:00347360
n3:jazykVysledku
n14:eng
n3:klicovaSlova
oxytocin analogues; deaminooxytocin; NMR
n3:klicoveSlovo
n11:oxytocin%20analogues n11:deaminooxytocin n11:NMR
n3:kodStatuVydavatele
AT - Rakouská republika
n3:kontrolniKodProRIV
[786FA1DC24B2]
n3:nazevZdroje
Amino Acids
n3:obor
n5:CC
n3:pocetDomacichTvurcuVysledku
2
n3:pocetTvurcuVysledku
7
n3:rokUplatneniVysledku
n7:2010
n3:svazekPeriodika
39
n3:tvurceVysledku
Fragiadaki, M. Slaninová, Jiřina Spyranti, Z. Magafa, V. Borovičková, Lenka Cordopatis, P. Spyroulias, G. A.
n3:wos
000279190400024
n3:zamer
n16:AV0Z40550506
s:issn
0939-4451
s:numberOfPages
10