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Statements

Subject Item
n2:RIV%2F61388963%3A_____%2F10%3A00346290%21RIV11-MSM-61388963
rdf:type
n3:Vysledek skos:Concept
dcterms:description
9-(2-Phosphonomethoxyethyl)-2,6-diamino-[8-3H]purine, 9-(2-phosphonomethoxyethyl)- [8-3H]guanine and (R)- 9-(2-phosphonomethoxypropyl)-[8-3H]adenine with specific activities of 10.9 Ci/mmol, 7.9 Ci/mmol and 16 Ci/mmol, respectively, were prepared by a catalytic dehalogenation of the corresponding 8-bromo derivatives. The rate of the exchange of the tritium label on C-8 of the purine ring in title compounds with the hydrogen of water under physiological pH at 20 °C was studied using 3H NMR. 9-(2-Phosphonomethoxyethyl)-2,6-diamino-[8-3H]purine, 9-(2-phosphonomethoxyethyl)- [8-3H]guanine and (R)- 9-(2-phosphonomethoxypropyl)-[8-3H]adenine with specific activities of 10.9 Ci/mmol, 7.9 Ci/mmol and 16 Ci/mmol, respectively, were prepared by a catalytic dehalogenation of the corresponding 8-bromo derivatives. The rate of the exchange of the tritium label on C-8 of the purine ring in title compounds with the hydrogen of water under physiological pH at 20 °C was studied using 3H NMR.
dcterms:title
The preparation of 3-H-labeled Acyclic Nucleoside Phosphonates and Study of their Stability The preparation of 3-H-labeled Acyclic Nucleoside Phosphonates and Study of their Stability
skos:prefLabel
The preparation of 3-H-labeled Acyclic Nucleoside Phosphonates and Study of their Stability The preparation of 3-H-labeled Acyclic Nucleoside Phosphonates and Study of their Stability
skos:notation
RIV/61388963:_____/10:00346290!RIV11-MSM-61388963
n5:aktivita
n13:Z n13:P
n5:aktivity
P(1M0508), P(IAA400550801), Z(AV0Z40550506)
n5:cisloPeriodika
7
n5:dodaniDat
n6:2011
n5:domaciTvurceVysledku
n16:2803852 n16:7989776 n16:9587217
n5:druhVysledku
n14:J
n5:duvernostUdaju
n9:S
n5:entitaPredkladatele
n18:predkladatel
n5:idSjednocenehoVysledku
281407
n5:idVysledku
RIV/61388963:_____/10:00346290
n5:jazykVysledku
n17:eng
n5:klicovaSlova
tritium; 3-H NMR; acyclic nucleotide analogues
n5:klicoveSlovo
n8:3-H%20NMR n8:tritium n8:acyclic%20nucleotide%20analogues
n5:kodStatuVydavatele
CZ - Česká republika
n5:kontrolniKodProRIV
[6AD1A1BD1E5B]
n5:nazevZdroje
Collection of Czechoslovak Chemical Communications
n5:obor
n7:CC
n5:pocetDomacichTvurcuVysledku
3
n5:pocetTvurcuVysledku
3
n5:projekt
n10:1M0508 n10:IAA400550801
n5:rokUplatneniVysledku
n6:2010
n5:svazekPeriodika
75
n5:tvurceVysledku
Holý, Antonín Břehová, Petra Elbert, Tomáš
n5:wos
000280518100004
n5:zamer
n15:AV0Z40550506
s:issn
0010-0765
s:numberOfPages
10