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Statements

Subject Item
n2:RIV%2F61388955%3A_____%2F10%3A00437045%21RIV15-AV0-61388955
rdf:type
skos:Concept n19:Vysledek
dcterms:description
The syntheses and structural characterizations of two novel 2-bromobenzoatozinc(II) complexes-[Zn(2-BrC6H4COO)(2)](n) (I) and [Zn(2-BrC6H4COO)(2)(mnad)](2) (II), where mnad is N-methylnicotinamide are reported. Compound (I) crystallized with a monoclinic lattice (space group P2(1)/c) and is polymeric in solid state. Its cell parameters are: a = 7.37220(10) angstrom, b = 19.9639(3) angstrom, c = 30.2756(5) angstrom, beta = 94.7510(7)degrees, V = 4440.59(12) angstrom(3), Z = 4. The coordination environments of all zinc atoms are distorted tetrahedra built from four carboxylate oxygen atoms coming from four 2-bromobenzoato ligands. Compound (II) crystallized with a monoclinic lattice (space group P2(1)/c) with a = 11.7488(2) angstrom, b = 20.3683(3) angstrom, c = 9.30130(10) angstrom, beta = 100.3941(11)degrees, V = 2189.30(5) angstrom(3), Z = 2. This dimeric molecule features a paddle-wheel [Zn2O8] cage in solid state; the coordination environment of the central atom is square pyramidal consisting of four carboxylate oxygen atoms and the pyridine N atom of the mnad ligand. The syntheses and structural characterizations of two novel 2-bromobenzoatozinc(II) complexes-[Zn(2-BrC6H4COO)(2)](n) (I) and [Zn(2-BrC6H4COO)(2)(mnad)](2) (II), where mnad is N-methylnicotinamide are reported. Compound (I) crystallized with a monoclinic lattice (space group P2(1)/c) and is polymeric in solid state. Its cell parameters are: a = 7.37220(10) angstrom, b = 19.9639(3) angstrom, c = 30.2756(5) angstrom, beta = 94.7510(7)degrees, V = 4440.59(12) angstrom(3), Z = 4. The coordination environments of all zinc atoms are distorted tetrahedra built from four carboxylate oxygen atoms coming from four 2-bromobenzoato ligands. Compound (II) crystallized with a monoclinic lattice (space group P2(1)/c) with a = 11.7488(2) angstrom, b = 20.3683(3) angstrom, c = 9.30130(10) angstrom, beta = 100.3941(11)degrees, V = 2189.30(5) angstrom(3), Z = 2. This dimeric molecule features a paddle-wheel [Zn2O8] cage in solid state; the coordination environment of the central atom is square pyramidal consisting of four carboxylate oxygen atoms and the pyridine N atom of the mnad ligand.
dcterms:title
Crystal Structure of [Zn(2-Bromobenzoato)(2)](n) and [Zn(2-Bromobenzoato)(2)(N-Methylnicotinamide)](2) Crystal Structure of [Zn(2-Bromobenzoato)(2)](n) and [Zn(2-Bromobenzoato)(2)(N-Methylnicotinamide)](2)
skos:prefLabel
Crystal Structure of [Zn(2-Bromobenzoato)(2)](n) and [Zn(2-Bromobenzoato)(2)(N-Methylnicotinamide)](2) Crystal Structure of [Zn(2-Bromobenzoato)(2)](n) and [Zn(2-Bromobenzoato)(2)(N-Methylnicotinamide)](2)
skos:notation
RIV/61388955:_____/10:00437045!RIV15-AV0-61388955
n3:aktivita
n6:P n6:Z
n3:aktivity
P(KAN100400701), Z(AV0Z40400503), Z(MSM0021620857)
n3:cisloPeriodika
8
n3:dodaniDat
n4:2015
n3:domaciTvurceVysledku
n11:5347440
n3:druhVysledku
n9:J
n3:duvernostUdaju
n12:S
n3:entitaPredkladatele
n8:predkladatel
n3:idSjednocenehoVysledku
252446
n3:idVysledku
RIV/61388955:_____/10:00437045
n3:jazykVysledku
n17:eng
n3:klicovaSlova
N-methylnicotinamide; Structural study; Zinc 2-bromobenzoate
n3:klicoveSlovo
n13:Zinc%202-bromobenzoate n13:N-methylnicotinamide n13:Structural%20study
n3:kodStatuVydavatele
US - Spojené státy americké
n3:kontrolniKodProRIV
[5D9FB68DB4D3]
n3:nazevZdroje
Journal of Chemical Crystallography
n3:obor
n18:CF
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
3
n3:projekt
n16:KAN100400701
n3:rokUplatneniVysledku
n4:2010
n3:svazekPeriodika
40
n3:tvurceVysledku
Krajniková, A. Gyepes, Robert Györová, K.
n3:wos
000279197600003
n3:zamer
n5:MSM0021620857 n5:AV0Z40400503
s:issn
1074-1542
s:numberOfPages
6
n10:doi
10.1007/s10870-010-9712-z