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Statements

Subject Item
n2:RIV%2F61388955%3A_____%2F09%3A00329272%21RIV10-MSM-61388955
rdf:type
n11:Vysledek skos:Concept
dcterms:description
A differential pulse voltammetric (DPV) method was developed for the determination of 4-nitrophenol (4-NP) at a newly developed silver amalgam paste electrode (AgA-PE) in Britton-Robinson buffer pH 3.0. The electrode is based on a disposable plastic pipette tip filled with paste amalgam based on a mixture of mercury and fine silver powder (9:1, w/w). The experimental parameters, such as pH of Britton-Robinson buffer and activation and regeneration potential of the electrode surface were optimized. The reduction peak current dependences were linear for the concentration of 4-NP from 0.2 to 100 mu M. The method showed reproducible results with RSD (n = 45) of 1.7%. The limit of determination (LOD) was 0.3 mu M. The method was successfully applied for the direct determination of 4-NP in drinking water. A differential pulse voltammetric (DPV) method was developed for the determination of 4-nitrophenol (4-NP) at a newly developed silver amalgam paste electrode (AgA-PE) in Britton-Robinson buffer pH 3.0. The electrode is based on a disposable plastic pipette tip filled with paste amalgam based on a mixture of mercury and fine silver powder (9:1, w/w). The experimental parameters, such as pH of Britton-Robinson buffer and activation and regeneration potential of the electrode surface were optimized. The reduction peak current dependences were linear for the concentration of 4-NP from 0.2 to 100 mu M. The method showed reproducible results with RSD (n = 45) of 1.7%. The limit of determination (LOD) was 0.3 mu M. The method was successfully applied for the direct determination of 4-NP in drinking water.
dcterms:title
Voltammetric Determination of 4-Nitrophenol Using a Novel Type of Silver Amalgam Paste Electrode Voltammetric Determination of 4-Nitrophenol Using a Novel Type of Silver Amalgam Paste Electrode
skos:prefLabel
Voltammetric Determination of 4-Nitrophenol Using a Novel Type of Silver Amalgam Paste Electrode Voltammetric Determination of 4-Nitrophenol Using a Novel Type of Silver Amalgam Paste Electrode
skos:notation
RIV/61388955:_____/09:00329272!RIV10-MSM-61388955
n3:aktivita
n7:Z n7:P
n3:aktivity
P(GA203/07/1195), P(LC06035), Z(AV0Z40400503), Z(MSM0021620857)
n3:cisloPeriodika
16
n3:dodaniDat
n4:2010
n3:domaciTvurceVysledku
Yosypchuk, Bogdan
n3:druhVysledku
n10:J
n3:duvernostUdaju
n5:S
n3:entitaPredkladatele
n17:predkladatel
n3:idSjednocenehoVysledku
349867
n3:idVysledku
RIV/61388955:_____/09:00329272
n3:jazykVysledku
n15:eng
n3:klicovaSlova
voltammetry; drinking water; silver amalgam paste electrode; 4-nitrophenol
n3:klicoveSlovo
n8:4-nitrophenol n8:voltammetry n8:silver%20amalgam%20paste%20electrode n8:drinking%20water
n3:kodStatuVydavatele
DE - Spolková republika Německo
n3:kontrolniKodProRIV
[6D97BBBCE0A0]
n3:nazevZdroje
Electroanalysis
n3:obor
n16:CG
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
6
n3:projekt
n13:LC06035 n13:GA203%2F07%2F1195
n3:rokUplatneniVysledku
n4:2009
n3:svazekPeriodika
21
n3:tvurceVysledku
Yosypchuk, Bogdan Bhanger, M. I. Fischer, J. Sirajuddin, C. Niaz, A. Barek, J.
n3:wos
000269425100003
n3:zamer
n9:AV0Z40400503 n9:MSM0021620857
s:issn
1040-0397
s:numberOfPages
6