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Statements

Subject Item
n2:RIV%2F60461373%3A22340%2F11%3A43877195%21RIV12-MSM-22340___
rdf:type
skos:Concept n9:Vysledek
dcterms:description
Surface-enhanced Raman scattering (SERS) and surface-enhanced infrared absorption (SEIRA) are powerful analytical techniques used for the study and characterization of ultrathin films and monolayers of organic compounds adsorbed on the nanostructured surface of several metals. The main requirement which has to be met for the SERS- and SEIRA-activity is the proper morphology of the surface in nano-scale, which can be tailored by the preparation procedure. In the present work different electrochemical preparation procedures of copper substrates (cathodic reduction from electrochemical baths or its combination with oxidation-reduction cycles (ORC) treatment) were developed with the aim of fabrication of the substrate with both SERS- and SEIRA-activity for the selected model analyte. The diffuse reflectance methodology was designed to study SEIRA-activity on large-scaled nanostructured surfaces. The nanostructure of the copper surface was characterized using Scanning Electron Microscopy (SEM). Surface-enhanced Raman scattering (SERS) and surface-enhanced infrared absorption (SEIRA) are powerful analytical techniques used for the study and characterization of ultrathin films and monolayers of organic compounds adsorbed on the nanostructured surface of several metals. The main requirement which has to be met for the SERS- and SEIRA-activity is the proper morphology of the surface in nano-scale, which can be tailored by the preparation procedure. In the present work different electrochemical preparation procedures of copper substrates (cathodic reduction from electrochemical baths or its combination with oxidation-reduction cycles (ORC) treatment) were developed with the aim of fabrication of the substrate with both SERS- and SEIRA-activity for the selected model analyte. The diffuse reflectance methodology was designed to study SEIRA-activity on large-scaled nanostructured surfaces. The nanostructure of the copper surface was characterized using Scanning Electron Microscopy (SEM).
dcterms:title
Spectroscopic study of SERS- and SEIRA-activity of copper large-scaled surface substrates prepared by electrochemical deposition: What is the role of oxidation-reduction cycle treatment? Spectroscopic study of SERS- and SEIRA-activity of copper large-scaled surface substrates prepared by electrochemical deposition: What is the role of oxidation-reduction cycle treatment?
skos:prefLabel
Spectroscopic study of SERS- and SEIRA-activity of copper large-scaled surface substrates prepared by electrochemical deposition: What is the role of oxidation-reduction cycle treatment? Spectroscopic study of SERS- and SEIRA-activity of copper large-scaled surface substrates prepared by electrochemical deposition: What is the role of oxidation-reduction cycle treatment?
skos:notation
RIV/60461373:22340/11:43877195!RIV12-MSM-22340___
n9:predkladatel
n10:orjk%3A22340
n3:aktivita
n16:S n16:P n16:Z
n3:aktivity
P(GD104/08/H055), S, Z(MSM6046137306), Z(MSM6046137307)
n3:cisloPeriodika
1
n3:dodaniDat
n20:2012
n3:domaciTvurceVysledku
n12:1098616 n12:8806640 n12:6761321 n12:3825361 n12:7290659 n12:6333729
n3:druhVysledku
n17:J
n3:duvernostUdaju
n19:S
n3:entitaPredkladatele
n21:predkladatel
n3:idSjednocenehoVysledku
231393
n3:idVysledku
RIV/60461373:22340/11:43877195
n3:jazykVysledku
n4:eng
n3:klicovaSlova
Principal component analysis (PCA); Scanning Electron Microscopy (SEM); Diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS); Surface-enhanced infrared absorption (SEIRA); Surface-enhanced Raman scattering (SERS)
n3:klicoveSlovo
n8:Scanning%20Electron%20Microscopy%20%28SEM%29 n8:Diffuse%20reflectance%20infrared%20Fourier%20transform%20spectroscopy%20%28DRIFTS%29 n8:Principal%20component%20analysis%20%28PCA%29 n8:Surface-enhanced%20Raman%20scattering%20%28SERS%29 n8:Surface-enhanced%20infrared%20absorption%20%28SEIRA%29
n3:kodStatuVydavatele
NL - Nizozemsko
n3:kontrolniKodProRIV
[D3AA389C400F]
n3:nazevZdroje
Journal of Molecular Structure
n3:obor
n18:CB
n3:pocetDomacichTvurcuVysledku
6
n3:pocetTvurcuVysledku
6
n3:projekt
n14:GD104%2F08%2FH055
n3:rokUplatneniVysledku
n20:2011
n3:svazekPeriodika
993
n3:tvurceVysledku
Kokaislová, Alžběta Čejková, Jitka Matějka, Pavel Člupek, Martin Prokopec, Vadym Dendisová, Marcela
n3:wos
000291066000064
n3:zamer
n11:MSM6046137307 n11:MSM6046137306
s:issn
0022-2860
s:numberOfPages
10
n6:doi
10.1016/j.molstruc.2010.11.019
n15:organizacniJednotka
22340