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Statements

Subject Item
n2:RIV%2F60461373%3A22330%2F10%3A00023844%21RIV11-MSM-22330___
rdf:type
skos:Concept n19:Vysledek
dcterms:description
Rapid, simple and cost-effective analytical methods with performance characteristics matching regulátory requirements are needed for effective control of occurrence of Fusarium toxins in cereals and cereal-based products to which they might be transferred during processing. Within this study, two alternative approaches enabling retrospective data analysis and identification of unknown signals in sample extracts have been implemented and validated for determination of 11 major Fusarium toxins. In both cases, ultra-high performance liquid chromatography (U-HPLC) coupled with high resolution mass spectrometry (HR MS) was employed. 13C isotopically labeled surrogates as well as matrix-matched standards were employed for quantification. As far as time of flight mass analyzer (TOF-MS) was a detection tool, the use of modified QuEChERS (quick easy cheap effective rugged and safe) sample preparation procedure, widely employed in multi-pesticides residue analysis, was shown as an optimal approach to obtain lo Rapid, simple and cost-effective analytical methods with performance characteristics matching regulátory requirements are needed for effective control of occurrence of Fusarium toxins in cereals and cereal-based products to which they might be transferred during processing. Within this study, two alternative approaches enabling retrospective data analysis and identification of unknown signals in sample extracts have been implemented and validated for determination of 11 major Fusarium toxins. In both cases, ultra-high performance liquid chromatography (U-HPLC) coupled with high resolution mass spectrometry (HR MS) was employed. 13C isotopically labeled surrogates as well as matrix-matched standards were employed for quantification. As far as time of flight mass analyzer (TOF-MS) was a detection tool, the use of modified QuEChERS (quick easy cheap effective rugged and safe) sample preparation procedure, widely employed in multi-pesticides residue analysis, was shown as an optimal approach to obtain lo
dcterms:title
Novel approaches in analysis of Fusarium mycotoxins in cereals employing ultra performance liquid chromatography coupled with high resolution mass spectrometry Novel approaches in analysis of Fusarium mycotoxins in cereals employing ultra performance liquid chromatography coupled with high resolution mass spectrometry
skos:prefLabel
Novel approaches in analysis of Fusarium mycotoxins in cereals employing ultra performance liquid chromatography coupled with high resolution mass spectrometry Novel approaches in analysis of Fusarium mycotoxins in cereals employing ultra performance liquid chromatography coupled with high resolution mass spectrometry
skos:notation
RIV/60461373:22330/10:00023844!RIV11-MSM-22330___
n4:aktivita
n13:P n13:Z
n4:aktivity
P(1B53043), P(2B08049), Z(MSM6046137305)
n4:cisloPeriodika
1
n4:dodaniDat
n9:2011
n4:domaciTvurceVysledku
n6:9241914 n6:4915917 n6:4389891 n6:7989253 n6:7726481 n6:8580588
n4:druhVysledku
n12:J
n4:duvernostUdaju
n8:S
n4:entitaPredkladatele
n18:predkladatel
n4:idSjednocenehoVysledku
275418
n4:idVysledku
RIV/60461373:22330/10:00023844
n4:jazykVysledku
n15:eng
n4:klicovaSlova
mycotoxins; cereals; high resolution mass spektrometry; QuEChERS
n4:klicoveSlovo
n7:cereals n7:QuEChERS n7:high%20resolution%20mass%20spektrometry n7:mycotoxins
n4:kodStatuVydavatele
NL - Nizozemsko
n4:kontrolniKodProRIV
[46A352A4B2F9]
n4:nazevZdroje
Anal.Chim.Acta
n4:obor
n16:GM
n4:pocetDomacichTvurcuVysledku
6
n4:pocetTvurcuVysledku
7
n4:projekt
n5:2B08049 n5:1B53043
n4:rokUplatneniVysledku
n9:2010
n4:svazekPeriodika
662
n4:tvurceVysledku
Godula, Michal Krplová, Alexandra Lacina, Ondřej Kostelanská, Marta Hajšlová, Jana Poustka, Jan Zachariášová, Milena
n4:wos
000275236200008
n4:zamer
n17:MSM6046137305
s:issn
0003-2670
s:numberOfPages
11
n14:organizacniJednotka
22330