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Statements

Subject Item
n2:RIV%2F60461373%3A22330%2F06%3A00017806%21RIV07-MSM-22330___
rdf:type
skos:Concept n14:Vysledek
dcterms:description
Potential of ultra-performance liquid chromatography (UPLC) separation strategy coupled with tandem (in space) mass spectrometric detection (MS/MS) in multiresidue pesticide analysis was critically assessed. Performance parameters such as number of theoretical plates, height of theoretical plate, peak symmetry and peak capacity were measured/calculated on the basis of data generated by analysis of apple extracts containing 17 (semi)polar pesticides representing various classes of active ingredients of widely used crop protective preparations. Ultra-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) procedure provided improved chromatographic parameters resulting in significantly increased sample throughput including lower solvent consumption and lower limits of quantitation (LOQs) for most of target analytes compared to common method employing conventional high-performance liquid chromatography (HPLC) separation. Potential of ultra-performance liquid chromatography (UPLC) separation strategy coupled with tandem (in space) mass spectrometric detection (MS/MS) in multiresidue pesticide analysis was critically assessed. Performance parameters such as number of theoretical plates, height of theoretical plate, peak symmetry and peak capacity were measured/calculated on the basis of data generated by analysis of apple extracts containing 17 (semi)polar pesticides representing various classes of active ingredients of widely used crop protective preparations. Ultra-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) procedure provided improved chromatographic parameters resulting in significantly increased sample throughput including lower solvent consumption and lower limits of quantitation (LOQs) for most of target analytes compared to common method employing conventional high-performance liquid chromatography (HPLC) separation. V článku je kriticky zhodnocena metoda extrémně účinné kapalinové chromatografie ve spojení s tandemovou hmotnostní spektrometrií (UPLC-MS/MS) v multireziduální analýze pesticidů. Parametry jako počet teoretických pater, výška teoretického patra, symetrie píku a kapacita píků byly měřeny pro 17 semipolárních pesticidů, které reprezentují různé skupiny aktivních složek ochranných prostředků plodin. Metoda UPLC-MS/MS poskytuje zlepšené chromatografické parametry, což zvyšuje produktivitu v sériové analýze včetně nižší spotřeby rozpouštědel a nižších kvantifikačních limitů ve srovnání s konvenční vysokoúčinnou kapalinovou chromatografií (HPLC).
dcterms:title
Ultra-Performance Liquid Chromatography - Tandem Mass Spectrometry (UPLC-MS/MS): A novel challenge in multiresidue pesticides analysis in food Ultra-Performance Liquid Chromatography - Tandem Mass Spectrometry (UPLC-MS/MS): A novel challenge in multiresidue pesticides analysis in food Extrémně účinná kapalinová chromatografie - tandemová hmotnostní spektrometrie (UPLC-MS/MS): Nová výzva v multireziduální analýze pesticidů v potravinách
skos:prefLabel
Ultra-Performance Liquid Chromatography - Tandem Mass Spectrometry (UPLC-MS/MS): A novel challenge in multiresidue pesticides analysis in food Extrémně účinná kapalinová chromatografie - tandemová hmotnostní spektrometrie (UPLC-MS/MS): Nová výzva v multireziduální analýze pesticidů v potravinách Ultra-Performance Liquid Chromatography - Tandem Mass Spectrometry (UPLC-MS/MS): A novel challenge in multiresidue pesticides analysis in food
skos:notation
RIV/60461373:22330/06:00017806!RIV07-MSM-22330___
n4:strany
8-17
n4:aktivita
n15:Z
n4:aktivity
Z(MSM6046137305)
n4:cisloPeriodika
1
n4:dodaniDat
n12:2007
n4:domaciTvurceVysledku
n7:9241914 n7:2217481 n7:8580588
n4:druhVysledku
n11:J
n4:duvernostUdaju
n13:S
n4:entitaPredkladatele
n6:predkladatel
n4:idSjednocenehoVysledku
504892
n4:idVysledku
RIV/60461373:22330/06:00017806
n4:jazykVysledku
n18:eng
n4:klicovaSlova
Ultra-performance liquid chromatography; High-performance liquid chromatography; Tandem mass spectrometry; Multiresidue; Pesticides; Food analysis
n4:klicoveSlovo
n8:Tandem%20mass%20spectrometry n8:Multiresidue n8:Ultra-performance%20liquid%20chromatography n8:High-performance%20liquid%20chromatography n8:Food%20analysis n8:Pesticides
n4:kodStatuVydavatele
NL - Nizozemsko
n4:kontrolniKodProRIV
[BFBF1BF97B0F]
n4:nazevZdroje
Anal.Chim.Acta
n4:obor
n17:CB
n4:pocetDomacichTvurcuVysledku
3
n4:pocetTvurcuVysledku
4
n4:rokUplatneniVysledku
n12:2006
n4:svazekPeriodika
577
n4:tvurceVysledku
Poustka, Jan Kovalczuk, Tomáš Hajšlová, Jana Jech, Martin
n4:zamer
n5:MSM6046137305
s:issn
0003-2670
s:numberOfPages
10
n16:organizacniJednotka
22330