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Statements

Subject Item
n2:RIV%2F60461373%3A22330%2F05%3A00016013%21RIV06-GA0-22330___
rdf:type
n10:Vysledek skos:Concept
dcterms:description
Stanovení oxohalogenidů v pitné vodě metodou on-line spojení kapilární isotachoforesa - zónová elektroforesa Some oxyhalides can be found in drinking waters as inorganic disinfection by-products. An on-line coupled capillary isotachophoresis - capillary zone electrophoresis (CITP-CZE) method was developed for the analysis of chlorate, chlorite and bromate in water. The optimized CITP-CZE electrolyte system consisted of the following: 10 mM - HCl + 20mM - -Alanine (leading electrolyte), 5 mM - succinic acid (terminating electrolyte), and 10 mM - succinic acid + 5 mM - -Alanine + 0.1 % HPMC (carrier electrolyte). A clear separation of oxyhalides from other components of drinking water was achieved within 25 min. Method characteristics, i.e., linearity (0-200 ng/mL), accuracy (88-110 %), intra-assay (3-5 %), quantification limit (5-15 ng/mL), and detection limit (2-5 ng/mL), were determined. Minimum labor requirements, sufficient sensitivity and low running cost are important attributes of this method. It was found that the developed method is useful for the routine analysis of oxyhalides in water. Some oxyhalides can be found in drinking waters as inorganic disinfection by-products. An on-line coupled capillary isotachophoresis - capillary zone electrophoresis (CITP-CZE) method was developed for the analysis of chlorate, chlorite and bromate in water. The optimized CITP-CZE electrolyte system consisted of the following: 10 mM - HCl + 20mM - -Alanine (leading electrolyte), 5 mM - succinic acid (terminating electrolyte), and 10 mM - succinic acid + 5 mM - -Alanine + 0.1 % HPMC (carrier electrolyte). A clear separation of oxyhalides from other components of drinking water was achieved within 25 min. Method characteristics, i.e., linearity (0-200 ng/mL), accuracy (88-110 %), intra-assay (3-5 %), quantification limit (5-15 ng/mL), and detection limit (2-5 ng/mL), were determined. Minimum labor requirements, sufficient sensitivity and low running cost are important attributes of this method. It was found that the developed method is useful for the routine analysis of oxyhalides in water.
dcterms:title
Stanovení oxohalogenidů v pitné vodě metodou on-line spojení kapilární isotachoforesa - zónová elektroforesa Determination of inorganic oxyhalides in drinking Determination of inorganic oxyhalides in drinking
skos:prefLabel
Determination of inorganic oxyhalides in drinking Stanovení oxohalogenidů v pitné vodě metodou on-line spojení kapilární isotachoforesa - zónová elektroforesa Determination of inorganic oxyhalides in drinking
skos:notation
RIV/60461373:22330/05:00016013!RIV06-GA0-22330___
n3:strany
137-145
n3:aktivita
n13:Z n13:P
n3:aktivity
P(GA525/03/0351), Z(MSM6046137305)
n3:cisloPeriodika
1
n3:dodaniDat
n15:2006
n3:domaciTvurceVysledku
n8:8995354 n8:9207309 n8:7992335 n8:1379496 n8:8936579
n3:druhVysledku
n18:J
n3:duvernostUdaju
n14:S
n3:entitaPredkladatele
n12:predkladatel
n3:idSjednocenehoVysledku
517596
n3:idVysledku
RIV/60461373:22330/05:00016013
n3:jazykVysledku
n4:eng
n3:klicovaSlova
Oxyhalides; drinking water; on-line coupled capillary isotachophoresis-zone electrophoresis
n3:klicoveSlovo
n5:Oxyhalides n5:drinking%20water n5:on-line%20coupled%20capillary%20isotachophoresis-zone%20electrophoresis
n3:kodStatuVydavatele
PL - Polská republika
n3:kontrolniKodProRIV
[25E6EE2A08F1]
n3:nazevZdroje
Central European Journal of Chemistry
n3:obor
n17:GM
n3:pocetDomacichTvurcuVysledku
5
n3:pocetTvurcuVysledku
5
n3:projekt
n9:GA525%2F03%2F0351
n3:rokUplatneniVysledku
n15:2005
n3:svazekPeriodika
3
n3:tvurceVysledku
Janda, Václav Kvasnička, František Manda, Jan Kollerová, Lubica Rousová, Daniela
n3:zamer
n19:MSM6046137305
s:issn
1644-3624
s:numberOfPages
9
n11:organizacniJednotka
22330