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Statements

Subject Item
n2:RIV%2F60461373%3A22310%2F14%3A43897456%21RIV15-GA0-22310___
rdf:type
n11:Vysledek skos:Concept
rdfs:seeAlso
http://www.sciencedirect.com/science/article/pii/S0040603114005498
dcterms:description
We synthesized and characterized (Bi0.4Sr0.6)Sr2CoO5?delta using X-ray diffraction (XRD) and scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS). In the next step the heat capacity and enthalpy increments of (Bi0.4Sr0.6)Sr2CoO5?delta were measured by physical property measurement system (PPMS), differential scanning calorimetry (DSC) and drop calorimetry. Oxygen non-stoichiometry was determined using thermogravimetric measurement (TG) and reduction in hydrogen atmosphere. Above room temperature the temperature dependence of the molar heat capacity in the form C pm = (201.0 + 0.09261 x T ? 2184097 x T ?2) J K?1 mol?1 was derived by the least squares method from the experimental data. The heat capacity was also analyzed in terms of a combined Debye-Einstein model. The molar entropy View the MathML sourceSm° (298.15) = 219.65 J mol?1 K?1 was evaluated from the low temperature heat capacity data We synthesized and characterized (Bi0.4Sr0.6)Sr2CoO5?delta using X-ray diffraction (XRD) and scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS). In the next step the heat capacity and enthalpy increments of (Bi0.4Sr0.6)Sr2CoO5?delta were measured by physical property measurement system (PPMS), differential scanning calorimetry (DSC) and drop calorimetry. Oxygen non-stoichiometry was determined using thermogravimetric measurement (TG) and reduction in hydrogen atmosphere. Above room temperature the temperature dependence of the molar heat capacity in the form C pm = (201.0 + 0.09261 x T ? 2184097 x T ?2) J K?1 mol?1 was derived by the least squares method from the experimental data. The heat capacity was also analyzed in terms of a combined Debye-Einstein model. The molar entropy View the MathML sourceSm° (298.15) = 219.65 J mol?1 K?1 was evaluated from the low temperature heat capacity data
dcterms:title
Structure, oxygen non-stoichiometry and thermal properties of (Bi0.4Sr0.6)Sr2CoO5-delta Structure, oxygen non-stoichiometry and thermal properties of (Bi0.4Sr0.6)Sr2CoO5-delta
skos:prefLabel
Structure, oxygen non-stoichiometry and thermal properties of (Bi0.4Sr0.6)Sr2CoO5-delta Structure, oxygen non-stoichiometry and thermal properties of (Bi0.4Sr0.6)Sr2CoO5-delta
skos:notation
RIV/60461373:22310/14:43897456!RIV15-GA0-22310___
n3:aktivita
n12:S n12:P
n3:aktivity
P(GA13-17538S), S
n3:cisloPeriodika
20 January 2015
n3:dodaniDat
n5:2015
n3:domaciTvurceVysledku
n4:1544632 n4:5250226 n4:6541690 n4:6562108 n4:3148262
n3:druhVysledku
n15:J
n3:duvernostUdaju
n18:S
n3:entitaPredkladatele
n19:predkladatel
n3:idSjednocenehoVysledku
47948
n3:idVysledku
RIV/60461373:22310/14:43897456
n3:jazykVysledku
n8:eng
n3:klicovaSlova
Thermogravimetry; Mixed oxides; Oxygen non-stoichiometry; Heat capacity
n3:klicoveSlovo
n7:Thermogravimetry n7:Heat%20capacity n7:Mixed%20oxides n7:Oxygen%20non-stoichiometry
n3:kodStatuVydavatele
NL - Nizozemsko
n3:kontrolniKodProRIV
[F20C73AA6A0B]
n3:nazevZdroje
Thermochimica Acta
n3:obor
n16:CA
n3:pocetDomacichTvurcuVysledku
5
n3:pocetTvurcuVysledku
7
n3:projekt
n13:GA13-17538S
n3:rokUplatneniVysledku
n5:2014
n3:svazekPeriodika
600
n3:tvurceVysledku
Svoboda, Pavel Vítek, Jindřich Šimek, Petr Sedmidubský, David Sofer, Zdeněk Jankovský, Ondřej Růžička, Květoslav
s:issn
0040-6031
s:numberOfPages
6
n14:doi
10.1016/j.tca.2014.12.002
n20:organizacniJednotka
22310