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Statements

Subject Item
n2:RIV%2F60461373%3A22310%2F06%3A00017008%21RIV07-MSM-22310___
rdf:type
n8:Vysledek skos:Concept
dcterms:description
The primary crystallization field of a perovskite solid solution Bi1−xSrxMnO3−gama was delimited by calculating the respective phase equilibria in the quaternary Bi-Sr-Mn-O system. The calculations are based on the recent assessment involving all three ternary subsystems, a quaternary liquid approximated as a mixture of Mn, MnO, Mn2O3, SrO and Bi2O3 species with binary Redlich-Kister coefficients and the perovskite phase described in terms of a point defect model allowing Sr2+ for Bi3+ substitution, oxygen vacancy formation and the related Mn3+/Mn4+ mixing on Mn-sublattice. The crystallization path and the composition of the crystallized solid solution are compared with single crystal growth experiments performed by self-flux method from a Bi-rich melt. The crystallization path obtained for a selected feed composition for which the largest and high quality single crystal have been grown, turns out to end very close to the global eutectic point. Primární krystalizační pole pevného roztoku perovskitu Bi1−xSrxMnO3−δ bylo určeno výpočtem příslušných fázových rovnováh v kvartérním systému Bi-Sr-Mn-O. The primary crystallization field of a perovskite solid solution Bi1−xSrxMnO3−gama was delimited by calculating the respective phase equilibria in the quaternary Bi-Sr-Mn-O system. The calculations are based on the recent assessment involving all three ternary subsystems, a quaternary liquid approximated as a mixture of Mn, MnO, Mn2O3, SrO and Bi2O3 species with binary Redlich-Kister coefficients and the perovskite phase described in terms of a point defect model allowing Sr2+ for Bi3+ substitution, oxygen vacancy formation and the related Mn3+/Mn4+ mixing on Mn-sublattice. The crystallization path and the composition of the crystallized solid solution are compared with single crystal growth experiments performed by self-flux method from a Bi-rich melt. The crystallization path obtained for a selected feed composition for which the largest and high quality single crystal have been grown, turns out to end very close to the global eutectic point.
dcterms:title
Single Crystal Growth of Bi1-xSrxMnO3 - Thermodynamics and Experiment Single Crystal Growth of Bi1-xSrxMnO3 - Thermodynamics and Experiment Růst monokrystalu Bi1-xSrxMnO3 - Termodynamika a experiment
skos:prefLabel
Single Crystal Growth of Bi1-xSrxMnO3 - Thermodynamics and Experiment Single Crystal Growth of Bi1-xSrxMnO3 - Thermodynamics and Experiment Růst monokrystalu Bi1-xSrxMnO3 - Termodynamika a experiment
skos:notation
RIV/60461373:22310/06:00017008!RIV07-MSM-22310___
n4:strany
38-41
n4:aktivita
n9:P n9:Z
n4:aktivity
P(GA203/03/0924), Z(MSM6046137302)
n4:cisloPeriodika
450
n4:dodaniDat
n6:2007
n4:domaciTvurceVysledku
n12:5094763 n12:1355686 n12:5395097 n12:6541690
n4:druhVysledku
n5:J
n4:duvernostUdaju
n16:S
n4:entitaPredkladatele
n11:predkladatel
n4:idSjednocenehoVysledku
499483
n4:idVysledku
RIV/60461373:22310/06:00017008
n4:jazykVysledku
n13:eng
n4:klicovaSlova
manganite perovskites; phase equilibria; thermodynamic modeling; single crystal growth
n4:klicoveSlovo
n10:phase%20equilibria n10:single%20crystal%20growth n10:thermodynamic%20modeling n10:manganite%20perovskites
n4:kodStatuVydavatele
NL - Nizozemsko
n4:kontrolniKodProRIV
[6C045BCF6C5D]
n4:nazevZdroje
Thermochimica Acta
n4:obor
n19:CA
n4:pocetDomacichTvurcuVysledku
4
n4:pocetTvurcuVysledku
4
n4:projekt
n17:GA203%2F03%2F0924
n4:rokUplatneniVysledku
n6:2006
n4:tvurceVysledku
Nevřiva, Miloš Sedmidubský, David Strejc, Aleš Leitner, Jindřich
n4:zamer
n15:MSM6046137302
s:issn
0040-6031
s:numberOfPages
4
n18:organizacniJednotka
22310