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Statements

Subject Item
n2:RIV%2F60162694%3AG44__%2F07%3A00001808%21RIV09-MO0-G44_____
rdf:type
n5:Vysledek skos:Concept
dcterms:description
Quaternary pyridinium aldoximes have been analyzed by thin-layer chromatography. Their separation was adequate when silica plates were used with a mobile phase with a high water content. As a consequence of their limited migration, reversed-phase TLC was not appropriate for determination of the lipophilicity of quaternary pyridinium aldoximes. Displacement TLC of some quaternary pyridinium aldoximes is, nevertheless, possible using silica as stationary phase with water-acetone-hydrochloric acid mobile phases. Normal-phase TLC with different concentrations of organic modifier gave a series of R M values for the pyridinium aldoximes. Approximation of the different plots of R M against organic modifier concentration to straight lines afforded R M,0 values and the slopes of the lines. The R M,0 values and the slopes both serve as indicators of the hydrophilic character of the compounds. Byla vyvinuta a v článku je popsána TLC metodika pro kvarterní inhibitory acetylcholinesterázy. Quaternary pyridinium aldoximes have been analyzed by thin-layer chromatography. Their separation was adequate when silica plates were used with a mobile phase with a high water content. As a consequence of their limited migration, reversed-phase TLC was not appropriate for determination of the lipophilicity of quaternary pyridinium aldoximes. Displacement TLC of some quaternary pyridinium aldoximes is, nevertheless, possible using silica as stationary phase with water-acetone-hydrochloric acid mobile phases. Normal-phase TLC with different concentrations of organic modifier gave a series of R M values for the pyridinium aldoximes. Approximation of the different plots of R M against organic modifier concentration to straight lines afforded R M,0 values and the slopes of the lines. The R M,0 values and the slopes both serve as indicators of the hydrophilic character of the compounds.
dcterms:title
TLC kvarternich pyridiniových aldoximů, antidot organofosforových estrerázových inhibitorů TLC of quaternary pyridinium aldoximes, antidotes of organophosphorus esterase inhibitors TLC of quaternary pyridinium aldoximes, antidotes of organophosphorus esterase inhibitors
skos:prefLabel
TLC of quaternary pyridinium aldoximes, antidotes of organophosphorus esterase inhibitors TLC of quaternary pyridinium aldoximes, antidotes of organophosphorus esterase inhibitors TLC kvarternich pyridiniových aldoximů, antidot organofosforových estrerázových inhibitorů
skos:notation
RIV/60162694:G44__/07:00001808!RIV09-MO0-G44_____
n3:aktivita
n9:Z
n3:aktivity
Z(MO0FVZ0000604)
n3:cisloPeriodika
1
n3:dodaniDat
n4:2009
n3:domaciTvurceVysledku
n15:6306888
n3:druhVysledku
n11:J
n3:duvernostUdaju
n8:S
n3:entitaPredkladatele
n13:predkladatel
n3:idSjednocenehoVysledku
455268
n3:idVysledku
RIV/60162694:G44__/07:00001808
n3:jazykVysledku
n18:eng
n3:klicovaSlova
Hydrophilicity; Pyridinium aldoximes; K-27; K-48
n3:klicoveSlovo
n7:K-48 n7:Hydrophilicity n7:Pyridinium%20aldoximes n7:K-27
n3:kodStatuVydavatele
HU - Maďarsko
n3:kontrolniKodProRIV
[FC682F09D80C]
n3:nazevZdroje
JPC-Journal of Planar Chromatography-Modern TLC
n3:obor
n17:FP
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
8
n3:rokUplatneniVysledku
n4:2007
n3:svazekPeriodika
20
n3:tvurceVysledku
Kalász, H. Kuča, Kamil Darvas, F. Laufer, R. Csermely, T. Gulyás, Z. Petroianu, G. Fürész, J.
n3:zamer
n10:MO0FVZ0000604
s:issn
0933-4173
s:numberOfPages
4
n12:organizacniJednotka
G44