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Statements

Subject Item
n2:RIV%2F60077344%3A_____%2F13%3A00397203%21RIV14-AV0-60077344
rdf:type
n4:Vysledek skos:Concept
dcterms:description
The possibilities of using a field emission scanning electron microscope (FESEM) equipped with an Autrata improved yttrium aluminum garnet (YAG) detector of back-scattered electrons (BSE) for a determination of metal nanoparticles sizes were examined in this study. The diameters of Au and Pd nanoparticles with different sizes were resolved based on digitally recorded FESEM micrographs and were compared with diameters obtained with a transmission electron microscope (TEM). In the case of Au nanoparticles, the data obtained from the FESEM exhibited smaller values in comparison with data from the TEM. The Pd nanoparticles diameters measured in the FESEM were comparable with those determined by means of the TEM, however. The influence of various parameters like the sizes of nanoparticles, their composition, use of accelerating voltage and other working conditions in the FESEM on the measurement results are discussed. The possibilities of using a field emission scanning electron microscope (FESEM) equipped with an Autrata improved yttrium aluminum garnet (YAG) detector of back-scattered electrons (BSE) for a determination of metal nanoparticles sizes were examined in this study. The diameters of Au and Pd nanoparticles with different sizes were resolved based on digitally recorded FESEM micrographs and were compared with diameters obtained with a transmission electron microscope (TEM). In the case of Au nanoparticles, the data obtained from the FESEM exhibited smaller values in comparison with data from the TEM. The Pd nanoparticles diameters measured in the FESEM were comparable with those determined by means of the TEM, however. The influence of various parameters like the sizes of nanoparticles, their composition, use of accelerating voltage and other working conditions in the FESEM on the measurement results are discussed.
dcterms:title
Is it possible to measure diameters of metal nanoparticles using BSE imaging in FESEM? Is it possible to measure diameters of metal nanoparticles using BSE imaging in FESEM?
skos:prefLabel
Is it possible to measure diameters of metal nanoparticles using BSE imaging in FESEM? Is it possible to measure diameters of metal nanoparticles using BSE imaging in FESEM?
skos:notation
RIV/60077344:_____/13:00397203!RIV14-AV0-60077344
n4:predkladatel
n16:ico%3A60077344
n6:aktivita
n11:V n11:P n11:I
n6:aktivity
I, P(GAP205/10/0348), P(KAN200520704), V
n6:cisloPeriodika
JAN 2013
n6:dodaniDat
n12:2014
n6:domaciTvurceVysledku
n9:4481062 n9:8966338 n9:6036813
n6:druhVysledku
n18:J
n6:duvernostUdaju
n7:S
n6:entitaPredkladatele
n10:predkladatel
n6:idSjednocenehoVysledku
81264
n6:idVysledku
RIV/60077344:_____/13:00397203
n6:jazykVysledku
n14:eng
n6:klicovaSlova
Au nanoparticles; Autrata YAG detector of BSE signal; FESEM; Pd nanoparticles; Size measurement
n6:klicoveSlovo
n13:Autrata%20YAG%20detector%20of%20BSE%20signal n13:FESEM n13:Pd%20nanoparticles n13:Size%20measurement n13:Au%20nanoparticles
n6:kodStatuVydavatele
GB - Spojené království Velké Británie a Severního Irska
n6:kontrolniKodProRIV
[1634AD9B6558]
n6:nazevZdroje
Micron
n6:obor
n17:EA
n6:pocetDomacichTvurcuVysledku
3
n6:pocetTvurcuVysledku
5
n6:projekt
n8:KAN200520704 n8:GAP205%2F10%2F0348
n6:rokUplatneniVysledku
n12:2013
n6:svazekPeriodika
44
n6:tvurceVysledku
Langhans, Jan Vancová, Marie Nebesářová, Jana Šlouf, Miroslav Pavlova, Ewa
n6:wos
000312925300015
s:issn
0968-4328
s:numberOfPages
8
n19:doi
10.1016/j.micron.2012.06.002