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Statements

Subject Item
n2:RIV%2F25794787%3A_____%2F11%3A%230000440%21RIV12-MSM-25794787
rdf:type
skos:Concept n16:Vysledek
rdfs:seeAlso
http://www.scientific.net/AMR.291-294.2914
dcterms:description
Our recent high resolution core level and valence level X-ray photoelectron spectra (XPS) of Natural-Styrene Butylene Rubber (NR/SBR) demonstrated much narrower linewidths than previously obtained on rubbers or other polymer coatings. This improvement is due to low-current, low-energy beam flood gun charge compensation on non-conductor rubbers. The different charging has compensated on the rough surface and in the bulk of sponge structure in depth 50 Å of rubber sample. Despite residual charging has occurred on the surface which is apparent in C1s and O1s shoulder on its right side of the peak shape. Carbon groups such as C-H, C-C, C=C cannot be easily differentiated by their principal C(1s) peak chemical shift. Carbon black fillers seem to behave quite differently in the rubber-curing reaction. The stability of vulcanized rubber with sulfur curing system was studied in components of C(1s), O(1s), S(2p) regions which represented appropriate estimation of changes of crosslinked with sulfide bonds on rubber surface. The connection between the Shore hardness of rubber and the presence of carbonyl and sulphonyl groups was apparent. A model has been proposed for the degradation of the crosslinking density of rubber after long term exposure. Our recent high resolution core level and valence level X-ray photoelectron spectra (XPS) of Natural-Styrene Butylene Rubber (NR/SBR) demonstrated much narrower linewidths than previously obtained on rubbers or other polymer coatings. This improvement is due to low-current, low-energy beam flood gun charge compensation on non-conductor rubbers. The different charging has compensated on the rough surface and in the bulk of sponge structure in depth 50 Å of rubber sample. Despite residual charging has occurred on the surface which is apparent in C1s and O1s shoulder on its right side of the peak shape. Carbon groups such as C-H, C-C, C=C cannot be easily differentiated by their principal C(1s) peak chemical shift. Carbon black fillers seem to behave quite differently in the rubber-curing reaction. The stability of vulcanized rubber with sulfur curing system was studied in components of C(1s), O(1s), S(2p) regions which represented appropriate estimation of changes of crosslinked with sulfide bonds on rubber surface. The connection between the Shore hardness of rubber and the presence of carbonyl and sulphonyl groups was apparent. A model has been proposed for the degradation of the crosslinking density of rubber after long term exposure.
dcterms:title
Evaluation of 18 Year-Service Lifetime of NR-SBR Lining Evaluation of 18 Year-Service Lifetime of NR-SBR Lining
skos:prefLabel
Evaluation of 18 Year-Service Lifetime of NR-SBR Lining Evaluation of 18 Year-Service Lifetime of NR-SBR Lining
skos:notation
RIV/25794787:_____/11:#0000440!RIV12-MSM-25794787
n16:predkladatel
n20:ico%3A25794787
n3:aktivita
n11:Z
n3:aktivity
Z(MSM2579478701)
n3:cisloPeriodika
2011
n3:dodaniDat
n19:2012
n3:domaciTvurceVysledku
n10:7127502 n10:8696500
n3:druhVysledku
n14:J
n3:duvernostUdaju
n6:S
n3:entitaPredkladatele
n15:predkladatel
n3:idSjednocenehoVysledku
198421
n3:idVysledku
RIV/25794787:_____/11:#0000440
n3:jazykVysledku
n17:eng
n3:klicovaSlova
hardness; lifetime; lining; NR; XPS surface analysis
n3:klicoveSlovo
n7:XPS%20surface%20analysis n7:lining n7:lifetime n7:NR n7:hardness
n3:kodStatuVydavatele
CH - Švýcarská konfederace
n3:kontrolniKodProRIV
[A875F7A0528A]
n3:nazevZdroje
Advanced Materials Research
n3:obor
n18:JK
n3:pocetDomacichTvurcuVysledku
2
n3:pocetTvurcuVysledku
2
n3:rokUplatneniVysledku
n19:2011
n3:svazekPeriodika
291-294
n3:tvurceVysledku
Kalabisová, Eva Racek, Jan
n3:zamer
n8:MSM2579478701
s:issn
1662-8985
s:numberOfPages
4
n13:doi
10.4028/www.scientific.net/AMR.291-294.2914