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Statements

Subject Item
n2:RIV%2F00216305%3A26210%2F12%3APU101656%21RIV13-MSM-26210___
rdf:type
n13:Vysledek skos:Concept
dcterms:description
Methods based on laser ablation, such as Laser Induced Breakdown Spectroscopy (LIBS) and Laser Ablation Inductively Coupled Plasma Mass/Optical Emission Spectrometry (LA-ICP-MS/OES) are particularly suitable for urinary stones bulk and micro analysis. The aim of this study is to demonstrate the calibration capabilities and limitations of these techniques. There are no commercially available standards, which would correspond to urinary calculi matrix. Internal standardization is also difficult, mainly due to different crystalline phases in one kidney stone. Calibration pellets were prepared from human urinary stones with phosphate, oxalate and urate matrix. For this comparative study the most frequently used laser-ablation based analytical techniques were chosen, such as LIBS and LA-ICP-MS. Moreover some unconventional techniques such as simultaneous LIBS – LA-ICP-OES and laser ablation (LA) – LIBS were also utilized. Methods based on laser ablation, such as Laser Induced Breakdown Spectroscopy (LIBS) and Laser Ablation Inductively Coupled Plasma Mass/Optical Emission Spectrometry (LA-ICP-MS/OES) are particularly suitable for urinary stones bulk and micro analysis. The aim of this study is to demonstrate the calibration capabilities and limitations of these techniques. There are no commercially available standards, which would correspond to urinary calculi matrix. Internal standardization is also difficult, mainly due to different crystalline phases in one kidney stone. Calibration pellets were prepared from human urinary stones with phosphate, oxalate and urate matrix. For this comparative study the most frequently used laser-ablation based analytical techniques were chosen, such as LIBS and LA-ICP-MS. Moreover some unconventional techniques such as simultaneous LIBS – LA-ICP-OES and laser ablation (LA) – LIBS were also utilized.
dcterms:title
Laser ablation Methods for Analysis of Urinary Stones: Comparison Study Based on Calibration Pellets Laser ablation Methods for Analysis of Urinary Stones: Comparison Study Based on Calibration Pellets
skos:prefLabel
Laser ablation Methods for Analysis of Urinary Stones: Comparison Study Based on Calibration Pellets Laser ablation Methods for Analysis of Urinary Stones: Comparison Study Based on Calibration Pellets
skos:notation
RIV/00216305:26210/12:PU101656!RIV13-MSM-26210___
n13:predkladatel
n15:orjk%3A26210
n3:aktivita
n10:P
n3:aktivity
P(ED1.1.00/02.0068), P(ME08002)
n3:dodaniDat
n4:2013
n3:domaciTvurceVysledku
n16:6620477
n3:druhVysledku
n9:O
n3:duvernostUdaju
n17:S
n3:entitaPredkladatele
n18:predkladatel
n3:idSjednocenehoVysledku
146472
n3:idVysledku
RIV/00216305:26210/12:PU101656
n3:jazykVysledku
n14:eng
n3:klicovaSlova
LIBS, Laser ablation, urinary stones, calibration pellets
n3:klicoveSlovo
n11:Laser%20ablation n11:LIBS n11:calibration%20pellets n11:urinary%20stones
n3:kontrolniKodProRIV
[8EE9E90F4814]
n3:obor
n12:CB
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
6
n3:projekt
n5:ME08002 n5:ED1.1.00%2F02.0068
n3:rokUplatneniVysledku
n4:2012
n3:tvurceVysledku
Kaiser, Jozef
n7:organizacniJednotka
26210