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Statements

Subject Item
n2:RIV%2F00216305%3A26210%2F08%3APU79866%21RIV10-MSM-26210___
rdf:type
skos:Concept n19:Vysledek
dcterms:description
Perovskite powders of the types La-Ca-Al-M-O , M = Fe, Cr, Mn, Co and La-Sr-Mn-Co-O were prepared via a sol-gel route according to the modified Pechini method. Incineration of the resins was performed before final sintering at 1273 K for 6 h. The phase composition of the samples was established by X-ray powder diffraction analysis, and the lattice parameters were calculated using Rietveld analysis. The shape and size of the particles were determined via scanning electron microscopy and the specific surface area of the powder perovskites was established by the BET method. The principal particles were ca. 100 nm in size and formed agglomerates larger than 1.0 lm. The composition of the perovskites was established by EDX analysis. Following this, the catalytic behavior was tested by means of total oxidation of propane. The catalytic performance was measured at atmospheric pressure with 3 g of catalyst in a fixed-bed quartz reactor (i.d. = 18 mm) under thermal-assisted and microwaveassisted conditions. In Perovskite powders of the types La-Ca-Al-M-O , M = Fe, Cr, Mn, Co and La-Sr-Mn-Co-O were prepared via a sol-gel route according to the modified Pechini method. Incineration of the resins was performed before final sintering at 1273 K for 6 h. The phase composition of the samples was established by X-ray powder diffraction analysis, and the lattice parameters were calculated using Rietveld analysis. The shape and size of the particles were determined via scanning electron microscopy and the specific surface area of the powder perovskites was established by the BET method. The principal particles were ca. 100 nm in size and formed agglomerates larger than 1.0 lm. The composition of the perovskites was established by EDX analysis. Following this, the catalytic behavior was tested by means of total oxidation of propane. The catalytic performance was measured at atmospheric pressure with 3 g of catalyst in a fixed-bed quartz reactor (i.d. = 18 mm) under thermal-assisted and microwaveassisted conditions. In
dcterms:title
Catalytic and Heating Behavior of Nanoscaled Perovskites under Microwave Radiation Catalytic and Heating Behavior of Nanoscaled Perovskites under Microwave Radiation
skos:prefLabel
Catalytic and Heating Behavior of Nanoscaled Perovskites under Microwave Radiation Catalytic and Heating Behavior of Nanoscaled Perovskites under Microwave Radiation
skos:notation
RIV/00216305:26210/08:PU79866!RIV10-MSM-26210___
n3:aktivita
n8:Z n8:P
n3:aktivity
P(OC 523.10), Z(MSM0021630508)
n3:cisloPeriodika
7
n3:dodaniDat
n9:2010
n3:domaciTvurceVysledku
n11:6883958
n3:druhVysledku
n12:J
n3:duvernostUdaju
n10:S
n3:entitaPredkladatele
n16:predkladatel
n3:idSjednocenehoVysledku
358927
n3:idVysledku
RIV/00216305:26210/08:PU79866
n3:jazykVysledku
n17:eng
n3:klicovaSlova
Heterogeneous catalysis, Nanoparticles, Oxidation, Perovskites
n3:klicoveSlovo
n7:Oxidation n7:Nanoparticles n7:Heterogeneous%20catalysis n7:Perovskites
n3:kodStatuVydavatele
DE - Spolková republika Německo
n3:kontrolniKodProRIV
[C5ED7F224F0C]
n3:nazevZdroje
CHEMICAL ENGINEERING & TECHNOLOGY
n3:obor
n18:JH
n3:pocetDomacichTvurcuVysledku
1
n3:pocetTvurcuVysledku
6
n3:projekt
n4:OC%20523.10
n3:rokUplatneniVysledku
n9:2008
n3:svazekPeriodika
31
n3:tvurceVysledku
Ondruschka, Bernd Krech, Thomas Moser, Christina Scholz, Peter Cihlář, Jaroslav Emmerich, Rudolf
n3:zamer
n14:MSM0021630508
s:issn
0930-7516
s:numberOfPages
6
n15:organizacniJednotka
26210